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•l _ <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell corn E-mail main@mccampbell corn <br /> Ground Zero Analysis,Inc Client Project ID #256,Gabbard Date Sampled 10/25-10/27/99 <br /> 1714 Main Street Date Received 10/29/99 <br /> Escalon,CA 95320 Client Contact John Lane Date Extracted 10/29/99 <br /> Client P O Date Analyzed 11/02-11/08/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 24356 <br /> Client ID GAB SB4-GW26 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<6 trans-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND Iodomethane ND <br /> Bromoform ND Isopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone ND <br /> sec-Butyl benzene ND Methylene Chloride` ND<2 <br /> tert-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide ND Methyl isobutyl ketones ND <br />• Carbon Tetrachloride ND Methyl tent-Butyl Ether(MTBE) — <br /> Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether") ND Styrene ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND<20 <br /> 4-Chlorotoluene ND Toluene"I ND <br /> Dibromochloromethane ND 1,2,3-Tnchlorobenzene ND <br /> 1,2-Dibrorno-3-chloropropane ND 1,2,4-Tnchlorobenzene ND <br /> Dibromomethane ND 1,1,1-Tnchloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Tnehloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichloroben7ene ND Tnchlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Tnchloropropane ND <br /> l,l-Dichloroethane ND 1,2,4-Tnmethylbenzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Tnmethylbenzene ND <br /> 1,1-Dichloroethene ND Vinyl Acetate ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride ° ND <br /> trans-1,2-Dichloroethene ND Xylenes,total ND <br /> 1,2-Dichloropropane ND Comments <br /> 1,3-Dichloropropane ND Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 102 <br /> 1,1-Dichloropropene ND Toluene-d8 1,07 <br /> cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 87 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in u91L <br /> Reporting limits unless otherwise stated water samples I ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/w1pe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br />. (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2 <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than--5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />