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110 2nd Ave South,ND7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htW Hwww mccampbell com E-mail main@mccampbell com <br /> i <br /> Ground Zero Analysts, Inc Client Project ID 4256, Gabbard Date Sampled 1/20/9 <br /> 1214 Main Street Date Received 01/21/99 <br /> Escalon, CA 95320 Client Contact John Lane Date Extracted 01/22-01/25/99 <br /> Client P O Date Analyzed 01/23-01/28/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 02128 <br /> Client ID GASB3-31GW } <br /> Matrix W 1 <br /> Compound Concentration* Compound Concentration* <br /> Acetone 110 Ethylbenzene 110 <br /> Benzene 180 Hexachlorobutadiene ND<17 <br /> Bromobenzene ND<17 lodomethane ND<17 <br /> Bromochloromethane ND<17 Isopropylbenzene ND<17 <br /> Bromodichloromethane ND<17 p-Isopropyl toluene ND<17 <br /> Bromoform ND<17 Methyl butyl ketone 44 <br /> Bromomethane ND<17 Methylene Chloride"' ND<l 10 <br /> n-Butyl benzene 21 Methyl ethyl ketone ND<17 <br /> sec-Butyl benzene ND<17 Methyl isobutyl ketone a 550 <br /> tert-Butyl benzene 35 Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<17 Naphthalene 680 <br /> Carbon Tetrachloride ND<17 n-Propyl benzene 33 <br /> Chlorobenzene ND<17 Styrene ND<17 <br /> Chloroethane ND<17 1,1,1,2-Tetracbloroethane ND<17 <br /> 2-Chloroethyl Vinyl Ether` ND<17 1,1,2,2-Tetrachloroethane ND<17 <br /> Chloroform ND<17 Tetrachloroethene ND<65 <br /> Chloromethane ND<17 Toluene ' 640 <br /> 2-Chlorotoluene ND<17 1,2,3-Tnchlorobenzene ND<17 <br /> 4-Chlorotoluene ND<17 1,2,4-Tnchlorobenzene ND<17 <br /> Dibromoehloromethane ND<17 1,1,1-Tnchloroethane ND<17 <br /> 1,2-Dibromo-3-chloropropane ND<17 1,1,2-Tnchloroethane ND<17 <br /> Dibromomethane ND<17 Tnchloroethene ND<17 <br /> 1,2-Dichlorobenzene 190 Trichlorofluoromethane ND<17 <br /> 1,3-Dichlorobenzene ND<17 1,2,3-Trichloropropane 170 <br /> 1,4-Dichlorobenzene 19 1,2,4-Tnmethylbenzene 270 <br /> Dichlorodifluoromethane ND<17 1,3,5-Tnmethylbenzene 97 <br /> l,l-Dichloroethane ND<17 Vinyl Acetate m ND<17 <br /> 1,2-Dicbloroethane ND<17 Vinyl Chloride ° ND<17 <br /> 1,1-Dichloroethene ND<17 Xylenes,total 570 <br /> cis-1,2-Dichloroethene ND<17 TPH-(g)(C6-C12) --- <br /> trans-1 2-Dichloroethene ND<17 TPH-(ms)(C8-C12) --- <br /> 1,2-Dichloropropane ND<17 TPH-(k)(C10+) --- <br /> 1,3-Dtchloropropane ND<17 <br /> 2,2-Dtchloropropane ND<17 Comments h <br /> I J-Dichloropropene ND<17 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<17 Dibromofluoromethane 97 <br /> trans-1,3-Dichloropropene ND<17 Toluene-d8 110 <br /> Ethylene dibromide ND<17 4-Bromofluorobenzene 97 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 0 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hanulton,Lab Director <br />