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Alpha Analytical, Inc. <br /> A255 Glendale Ave •Suite 21 -Sparks,Nevada 89431-5778 <br /> (775) 355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> *Date Work Order <br /> 12-Jan-03 W Summary Report 02120922 <br /> Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID D kHPCHEMkMSOMDATAk021211102121106 D Batch ID MS8W1211A Analysis Date 12/11/2002 13 14 <br /> Sample ID MBLK MS8W1211A Units NgIL Run ID GCIMSD_8_021211A Prep Date 12/11/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> Tertiary 9utyl Alcohol(TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 05 <br /> Di-isopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 1 <br /> 1,2-Dichloroethane ND 1 <br /> Benzene ND 0 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 0 5 <br /> 1 2-Dibromoethane(EDB) ND 2 <br /> Ethylbenzene ND 05 <br /> m,p-Xylene ND 0 5 <br /> o-Xylene ND 0 5 <br /> Surr 1,2-Dichloroethane-d4 9 66 10 97 71 130 <br /> Surr Toluene-d8 9 64 10 96 69 127 <br /> Surr 4-Bromofluorobenzene 107 10 107 80 123 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> File ID D 1HPCHEMIMSOBIDATA1021211102121103 D Batch ID MS8W1211A Analysis Date 12/1112002 12 06 <br /> Sample ID LCS MSBW1211A Units pg1L Run ID GCIMSD_B_021211A Prep Date 1211112002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> Benzene 11 0 5 10 110 80 120 <br /> Toluene 954 0 5 10 95 80 120 <br /> methylbenzene 103 0 5 10 103 80 120 <br /> p-Xylene 21 5 0 5 20 107 73 129 <br /> o-Xylene 11 0 5 10 110 73 127 <br /> Surr 1 2-DFchloroethane-d4 103 10 103 71 130 <br /> Surr Toluene-d8 935 10 94 69 127 <br /> Surr 4-Bromofluorobenzene 109 10 109 80 123 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D kHPCHEM1MS081DATA`021211102121108 D Batch ID MSBW1211A Analysis Date 12/11/2002 14 00 <br /> Sample ID 02120926-01AMS Units pg1L Run ID GCIMSD_B 021211A Prep Date 12/11/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qua] <br /> Benzene 579 1 3 50 0 116 80 120 <br /> Toluene 484 1 3 50 0 97 80 120 <br /> Ethylbenzene 529 1 3 50 0 106 80 120 <br /> m p-Xylene 103 1 3 100 0 103 73 129 <br /> o-Xylene 52 3 1 3 50 0 105 73 127 <br /> Surr 1,2-Dichloroethane-d4 487 50 97 71 130 <br /> Surr Toluene-d8 456 50 91 69 127 <br /> Surr 4-Bromofluorobenzene 51 9 50 104 80 123 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> File ID D 1HPCHEMkMS081DATA1021211102121109 D Batch 1D MSBW1211A Analysis Date 12/11/2002 14 22 <br /> Sample ID 02120926-01AMSD Units NgIL Run ID GCIMSD_8_021211A Prep Date 12/1112002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-irmt RPD Ref Val %RPD Qua] <br /> Benzene 59 1.3 50 0 118 80 120 5786 1 9 - <br /> Toluene 51 1 3 50 0 102 80 120 4841 521 <br /> Ethylbenzene 544 13 50 0 109 80 120 5288 282 <br /> m p-Xylene 106 1 3 100 0 106 73 129 1028 2 86 <br /> o-Xylene 534 1 3 50 0 107 73 127 5227 2 1 <br /> Surr 1 2-Dichloroethane-d4 492 50 98 71 130 <br /> Surr Toluene-d8 475 50 95 69 127 <br /> �rr 4-Bromofluorobenzene 55 50 110 80 123 <br /> 1 <br />