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f fir,. Lancaster <br />• <br />- Laboratories <br />2426 New HollaiW Pike. PO Box 12425, Lancaster, PA 17605-2425 -717 8513•2800 Fax: 717-656-2681 • WWW.ianca51eTi3bSZOnl <br />Analysis Re <br />Quality Control Summary <br />*- Outside of specification <br />The result for one or both deterrninations was less than five tines the LOQ. <br />t-1 The background result was more than four limes the spike added. <br />i. <br />i <br />Page I of 3 <br />RPD RPD Max <br />DUP Dup <br />RPD <br />JRPD Max <br />Client Name: ChevronTexaco <br />Group Number: <br />849104 <br />Reported: 05/05/03 at 08:56 <br />AM <br />Laboratory Compliance <br />Quality <br />Control <br />Dlank Blank Report <br />LC5 LCSD <br />LCS/LCSD <br />Analy6ie Name <br />Result MDL Unita <br />%REC %REC <br />Limits <br />Batch number: 03112A07D <br />Sample number(s): 40310224031025 <br />TPR-GRO - Waters <br />N.D- 50, ug/1 <br />109 <br />70-130 <br />Batch number: 03113A07A <br />Sample number(s)c 4031026 <br />TPH-GRO - Waters <br />N.D. 50. Ug/l <br />92 <br />70-130 <br />Batch number: U31140019A <br />Sample number(S): 4031022-4031025 <br />Methanol (by Direct Injection) <br />N.D. 200. ug/l <br />96 <br />78-114 <br />Batch number. P031122AA <br />Sample number(s): 4031022-4031026 <br />'-� <br />Ethanol <br />Methyl Tertiary Butyl Ether <br />N.D_ 50. ug/1 <br />N.D. .5 ug/l <br />113 <br />100 <br />43-159 <br />77-127 <br />di -Isopropyl ether <br />N -D. .5 119/1 <br />99 <br />74-125 <br />Ethyl t -butyl ether <br />N.D. .5 ug/I <br />100 <br />74-120 <br />-.1 <br />t -Amyl methyl ether <br />N.D. .5 ug/1 <br />99 <br />79-113 <br />t -Butyl alcohol <br />N.D_ 5. ug/l <br />106 <br />53-147 <br />Benzene <br />N.D. .5 ug/l <br />102 <br />85-117 <br />1,2-Dichloroethane <br />N.D. .5 ug/l <br />99 <br />77-132 <br />-q:'-�luene <br />N.D. .5 ug/l <br />101 <br />85-115 <br />'Q-Dibromoethane <br />N.D. .5 u9/1 <br />99 <br />81-114 <br />��hylbenzene <br />N.D. 5 ug/1 <br />99 <br />82-119 <br />Xylene (Total) <br />N.D. ,5 ug/l <br />99 <br />84-120 <br />Sample Matrix <br />Quality Control <br />MS XSD MS/MSD <br />RPD EKG <br />DUP <br />Analysis Name <br />%REC %REC Limits RPD MAX Conc <br />cone <br />Batch number: 03112A07D <br />Sample number(s): 4031022-4031025 <br />TPH-GRO - Waters <br />115 105 70-130 8 <br />30 <br />Batch number: 03113A07A <br />Sample number(s): 4031026 <br />TPN-GRO - Waters <br />107 108 70-130 1 <br />30 <br />Batch number: 032140019A <br />Sample number(s): 4031022-4031025 <br />Methanol (by Direct Injection) <br />92 92 78-116 0 <br />20 <br />Batch number: P021122AA <br />Sample number(s): 4031022-4031026 <br />Ethanol <br />126 133 34-163 5 <br />30 <br />r'sl <br />Methyl Tertiary Butyl Ether <br />105 107 69-134 1 <br />30 <br />!-1 <br />di -Isopropyl ether <br />105 107 75-130 2 <br />30 <br />Ethyl t -butyl ether <br />105 105 73-123 0 <br />30 <br />t -Amyl methyl ether <br />106 108 77-117 2 <br />30 <br />t -Butyl alcohol <br />113 116 39-155 2 <br />30 <br />Benzene <br />112 112 83-128 1 <br />30 <br />1,2-Dichloroethane <br />105 106 73-136 1 <br />3n <br />Toluene <br />106 109 83-127 2 <br />30 <br />1,2-Dibromoethane <br />100 103 78-120 3 <br />30 <br />Ethylbenzene <br />105 109 82-134 4 <br />30 <br />Xylene (Total) <br />106 109 82-130 3 <br />30 <br />*- Outside of specification <br />The result for one or both deterrninations was less than five tines the LOQ. <br />t-1 The background result was more than four limes the spike added. <br />i. <br />i <br />Page I of 3 <br />RPD RPD Max <br />DUP Dup <br />RPD <br />JRPD Max <br />