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Lancaster <br />Laboratories <br />Lancaster Laboratories Sample No. WW <br />Collected:06/05/2003 09:40 by ST <br />Submitted: 06/07/2003 10:15 <br />'i Reported: 06/23/2003 at 11:49 <br />Discard: 07/24/2003 <br />EFFL Grab Water Sample <br />Facility## 95775 <br />301 W- Kettleman Lane - Lodi, CA <br />EFF31 <br />4065001 <br />Page I of l <br />Account Number: 10869 <br />ChevronTexaco <br />6001 Bollinger Canyon Rd L4310 <br />San Ramon CA 94583 <br />As Received <br />CAT As Received Method Dilution <br />No. Analysis Name CAS Number Result Detection Units Factor <br />Limit <br />01728 TPH-GRO - Waters n -a. N.D. 50- ug/l 1 <br />The reported concentration of TPH-GRO does not include MTBE or other <br />gasoline constituents eluting prior to the C6 fn -hexane► TPH-GRO range <br />start time - <br />A site-specific MSD sample was not submitted for the project. A LCS/LCSD <br />was performed to demonstrate precision and accuracy at a batch level - <br />01412 Methanol and Ethanol <br />Methanol (by Direct Injection} 67-56-1 <br />N -D. <br />400. <br />ug/l <br />1 <br />.J <br />01594 <br />BTER + Oxygenates by 8260B <br />41587 <br />Ethanol 64-17-5 <br />N.D. <br />100- <br />ug/l <br />1 <br />02010 <br />Methyl Tertiary Butyl Ether 1634-04-4 <br />N.D. <br />2. <br />ug/l <br />1 <br />02011 <br />di -Isopropyl ether 108-20-3 <br />N.D- <br />2- <br />ug/1 <br />1 <br />02013 <br />Ethyl t -butyl ether 637-92-3 <br />N.D. <br />2. <br />ug/l <br />1 <br />02014 <br />t -Amyl methyl ether 994-05-6 <br />N.D- <br />2. <br />ug/l <br />1 <br />02015 <br />t -Butyl alcohol 75-65-0 <br />N.D- <br />10- <br />ug/1 <br />1 <br />05401 <br />Benzene 71-43-2 <br />N.D- <br />2. <br />ug/1 <br />1 <br />05402 <br />1,2-Dichloroethane 107-06-2 <br />N.D- <br />2. <br />ug/1 <br />1 <br />05407 <br />Toluene 108-88-3 <br />N.D- <br />2, <br />ug/1 <br />1 <br />05412 <br />1,2-Dibromoethane 106-93-4 <br />N.D- <br />2. <br />ug/1 <br />1 <br />05415 <br />Ethylbenzene 100-41-4 <br />N.D- <br />2. <br />ug/1 <br />1 <br />06310 <br />i <br />Xylene (Total) 1330-20-7 <br />N.D- <br />2. <br />ug/1 <br />1 <br />State of California Lab Certification No. 2116 <br />i <br />Laboratory <br />Chronicle <br />CAT <br />Analysis <br />Dilution <br />No. <br />Analysis Name Method <br />Trial# <br />Date and Time <br />Analyst <br />Factor <br />01728 <br />TPH-GRO - Waters N. CA LUFT Gasoline <br />1 <br />06/17/2003 <br />10:44 <br />Michael <br />F Barrow <br />1 <br />Method <br />01412 <br />Methanol and Ethanol SW -846 8015B <br />1 <br />06/19/2003 <br />11:20 <br />Lisa A <br />Johnson <br />1 <br />01594 <br />BTER + Oxygenates by 6260B SW -846 8260B <br />1 <br />06/18/2003 <br />11:18 <br />John B <br />Kiser <br />1 <br />01146 <br />GC VOA Water Prep SW -846 5030B <br />1 <br />06/17/2003 <br />10:44 <br />Michael <br />F Barrow <br />n.a. <br />„t',1163 <br />GC/MS VOA Water Prep SW -846 50308 <br />1 <br />06/18/2003 <br />11:18 <br />John B <br />Kiser <br />n.a. <br />Lancaster Laboratories, Inc. <br />2425 New Holland Pike <br />M E M S R <br />PO Bow 1 <br />� Lancaster,r, PA PA 17605-2425 <br />717-656-2300 Fix, 717-6562681 <br />2716 Rev. 3/10/03 <br />