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Lancaster.raor <br />Laboratories <br />Quality Control Summary <br />Surrogate Quality Control <br />Analysis Name: TPH-GRO - Waters <br />Batch number: 0316BA078 <br />*- Outside of specification <br />l The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />F. <br />l <br />Client Name: ChevronTexaco <br />' MEMBER <br />Group Number: <br />655926 <br />717-656-2300 Fax: 717-67-6 56-2681 <br />Reported: 06/23/03 at 11:50 AM <br />Laboratory <br />Compliance Quality <br />Control <br />Blank <br />Blank Report LCS LCSD <br />LCS/LCSD <br />Analysis Name <br />Result <br />MDL Units %RFC %REC <br />Limits <br />Batch number: 0316BA07B <br />Sample <br />number(s): 4065001-4065005 <br />70-130 <br />TPH-GRO - Waters <br />N.D. <br />50. ug/1 100 104 <br />{ <br />Batch number: 031700001A <br />Sample <br />number(s): 4065001-4065005 <br />Methanol (by Direct Injection) <br />N.D. <br />200. ug/l 100 <br />78-114 <br />Batch number: P031672AB <br />Sample <br />number{s): 4065001-4065005 <br />50- ug/1 52 <br />43-159 <br />♦ <br />Ethanol <br />N -D. <br />Methyl Tertiary Butyl Ether <br />N.D. <br />0.5 ug/1 97 <br />77-127 <br />74-125 <br />di -Isopropyl ether <br />N.D. <br />0.5 ug/1 101 <br />0.5 ug/l 101 <br />74-120 <br />Ethyl t -butyl ether <br />N.D. <br />0.5 ug/l 98 <br />79-113 <br />t -Amyl methyl ether <br />N.D. <br />N.D. <br />5. ug/l 65 <br />53-147 <br />r <br />t -Butyl alcohol <br />N.D. <br />0.5 ug/l 108 <br />65-117 <br />Benzene <br />1,2-D1chloroethane <br />N.D. <br />0.5 u9/1 103 <br />77-132 <br />Toluene <br />N.D. <br />0.5 ug/1 98 <br />85-115 <br />1,2-Dibromoethane <br />N.D. <br />0.5 u9/1 91 <br />81-119 <br />Ethylbenzene <br />N.D. <br />0.5 ug/l 98 <br />62 119 <br />Xylene (Total) <br />N.D. <br />0.5 ug/l 98 <br />84-120 <br />F ,tel <br />� <br />Sample Matrix Quality Control <br />MS <br />MSD MS/MSD RPD BKG <br />DUP <br />Analysis -Name <br />%REC <br />%REC Limits RPD MAX Conc <br />Conc <br />Batch number: 0316BA07B <br />Sample <br />number(s): 4065001-4065005 <br />TPH-GRO - Waters <br />105 <br />70-130 <br />r <br />Batch number: 031700001A <br />Methanol (by Direct Injection) <br />Sample <br />100 <br />number(s): 4065001-4065005 <br />96 78-116 4 20 <br />Batch number: P031672AB <br />Sample <br />number(s): 4065001-4065005 <br />Ethanol <br />52 <br />87 34-163 511 30 <br />Methyl Tertiary Butyl Ether <br />di -Isopropyl ether <br />99 <br />105 <br />98 69-134 2 30 <br />102 75-130 2 30 <br />Ethyl t -butyl ether <br />104 <br />102 73-123 1 30 <br />t -Amyl methyl ether <br />102 <br />100 77-117 3 30 <br />t -Butyl alcohol <br />65 <br />83 39-155 24 30 <br />` <br />Benzene <br />1,2-Dichloroethane <br />115 <br />104 <br />113 83-128 1 30 <br />103 73-136 0 30 <br />Toluene <br />106 <br />106 83-127 2 30 <br />1,2-Dibromoethane <br />95 <br />92 78-120 3 30 <br />Ethylben2ene <br />107 <br />104 82-134 3 30 <br />k + <br />Xylene (Total) <br />106 <br />105 82-130 1 30 <br />Surrogate Quality Control <br />Analysis Name: TPH-GRO - Waters <br />Batch number: 0316BA078 <br />*- Outside of specification <br />l The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />F. <br />l <br />Page f of 2 <br />RPD RPD Max <br />4 <br />DUP <br />RPD <br />30 <br />Dup <br />RPD <br />Max <br />1216 Rev. 3/10103 <br />Lancaster Laboratories, Inc. <br />' MEMBER <br />2425 New Holland Pike <br />PO Box 12425 <br />Lancaster, PA 17605-2425 <br />1 <br />717-656-2300 Fax: 717-67-6 56-2681 <br />Page f of 2 <br />RPD RPD Max <br />4 <br />DUP <br />RPD <br />30 <br />Dup <br />RPD <br />Max <br />1216 Rev. 3/10103 <br />