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Lancaster <br />Laboratories <br />Quality Control Summary <br />Client Name: ChevronTexaco <br />Reported: 01/02/03 at 03:52 PM <br />Analvsis Name <br />Batch number: 023460023A <br />Methanol (by Direct Injection) <br />Batch number: N023441AA <br />Ethanol <br />Methyl t -butyl ether <br />di -Isopropyl ether <br />Ethyl t -butyl ether <br />t -Amyl methyl ether <br />t -Butyl alcohol <br />Benzene <br />1,2-Dichloroethane <br />Toluene <br />1,2-Dibromoethane <br />Ethylbenzene <br />X leve (Total) <br />`.ch number: N023442AA <br />Ethanol <br />Methyl t --butyl ether <br />di -Isopropyl ether <br />Ethyl t -butyl ether <br />t -Amyl methyl ether <br />t -Butyl alcohol <br />Benzene <br />1,2-Dichloroethane <br />Toluene <br />1,2-Dibromoethane <br />Ethylbenzene <br />Xylene (Total) <br />Analysis Name: TPH-GRO - Waters <br />Batch number: 02343A16A <br />Trifluorotoluene-F <br />3955354 110 <br />3955355 110 <br />3955356 107 <br />REPRINT <br />Group Number: 833534 <br />Sample Matrix Quality Control <br />MS <br />MSD <br />MS/MSD <br />RPD <br />%REC <br />%REC <br />Limits <br />RPD <br />MAX <br />Sample <br />number(s): 3955354-3955357 <br />88 <br />85 <br />69-127 <br />4 <br />20 <br />Sample <br />number(s): 3955354 <br />91 <br />91 <br />34-163 <br />0 <br />30 <br />92 <br />93 <br />69-134 <br />1 <br />30 <br />94 <br />95 <br />68-133 <br />1 <br />30 <br />104 <br />106 <br />73-123 <br />1 <br />30 <br />98 <br />99 <br />69-118 <br />2 <br />30 <br />112 <br />113 <br />51-148 <br />1 <br />30 <br />111 <br />111 <br />78-134 <br />0 <br />30 <br />94 <br />94 <br />73-136 <br />0 <br />30 <br />109 <br />107 <br />83-127 <br />2 <br />30 <br />105 <br />104 <br />78-120 <br />1 <br />30 <br />106 <br />106 <br />82-134 <br />1 <br />30 <br />109 <br />108 <br />82-130 <br />1 <br />30 <br />Sample <br />number(s): <br />3955355-3955358 <br />83 <br />78 <br />34-163 <br />5 <br />30 <br />92 <br />89 <br />69-134 <br />3 <br />30 <br />89 <br />87 <br />68-133 <br />3 <br />30 <br />102 <br />100 <br />73-123 <br />2 <br />30 <br />95 <br />93 <br />69-118 <br />2 <br />30 <br />104 <br />101 <br />51-148 <br />2 <br />30 <br />108 <br />106 <br />78-134 <br />3 <br />30 <br />96 <br />94 <br />73-136 <br />2 <br />30 <br />109 <br />106 <br />83-127 <br />3 <br />30 <br />105 <br />102 <br />78-120 <br />3 <br />30 <br />107 <br />104 <br />82-134 <br />3 <br />30 <br />108 <br />105 <br />82-130 <br />3 <br />30 <br />BKG DUP <br />Can¢ Cone <br />Surrogate Quality Control <br />*- Outside of specification <br />( 1) The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />a <br />Lancaster Laboratories, Inc. <br />M B M B B R 2425 New Holland Pike <br />®PO Box 12425 <br />Lancaster, PA 17605.2425 <br />717-656-2300 Fax: 717-656.2681 <br />Page 2 of 4 <br />DUP Dup <br />RPD <br />RPD Max <br />2216 Rev. 10/2102 <br />