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fdILLancaster <br />Laboratories ort <br />Analysis Re <br />24226 ►f7,,, Halyr,d Pte. �+C Bx ,2a85, Leu ra,eid�. N , <br />xhosz+z5•xrr45�2,00 Fad r,r 2na,•wwwJaXA61arfats com <br />Page 2 of 3 <br />Quality Control Summary. <br />Client Name: ChevronTexaco <br />Reported: 05/20/04 at 04:48 PM Group Number: 895826 <br />Sample Matrix Quality Control <br />Analysis Nesme MS MSD HS/KSD APD BKG DUP <br />ABC REC Limits RPD DUP Dup RPD <br />Batch number: 0413SA086 � Capo Conc RPD MAX <br />TPH-GRO - Waters Sample number(s): 4272160-4272162 <br />129 63-154 <br />Batch number: P041382AA <br />Ethanol <br />Methyl Tertiary Butyl Ether <br />di -Isopropyl ether <br />Ethyl t -butyl ether <br />t -Amyl methyl ether <br />t -Butyl alcohol <br />Benzene <br />1,2-Dichloroethane <br />Toluene <br />1,2-Dibromoethane <br />Ethylbenzene <br />Xylene (Total) <br />Batch number: P041392AB <br />Ethanol <br />Methyl Tertiary Butyl Ether <br />di-rsopropyl ether <br />Ethyl t -butyl ether <br />t -Amyl methyl ether <br />t -Butyl alcohol <br />Benzene <br />1,2 -Di chloroethane <br />Toluene <br />1,2-Dibromoethane <br />Ethylbenzene <br />Xylene (Total) <br />Analysis Name! TPH-CRO - Waters <br />Sample <br />number(s): 4272159-4272160 <br />94 <br />92 <br />41-155 <br />2 <br />30 <br />107 <br />106 <br />69-134 <br />1 <br />30 <br />95 <br />94 <br />75-130 <br />1 <br />30 <br />99 <br />97 <br />78-119 <br />2 <br />30 <br />106 <br />107 <br />77-117 <br />1 <br />30 <br />113 <br />113 <br />51-147 <br />0 <br />30 <br />104 <br />102 <br />83-128 <br />2 <br />30 <br />108 <br />106 <br />73-136 <br />0 <br />30 <br />102 <br />102 <br />83-127 <br />0 <br />30 <br />97 <br />96 <br />78-120 <br />1 <br />30 <br />105 <br />103 <br />82-129 <br />1 <br />30 <br />105 <br />103 <br />82-130 <br />2 <br />30 <br />Sample <br />number(s): 4272161-4272162 <br />81 <br />77 <br />41-155 <br />6 <br />30 <br />105 <br />110 <br />69-134 <br />3 <br />30 <br />78 <br />80 <br />75-130 <br />3' <br />30. <br />89 <br />91 <br />78-119 <br />3 <br />30 <br />101 <br />105 <br />77-117 <br />4 <br />30 <br />105 <br />103 <br />51-147 <br />2 <br />30 <br />97 <br />100 <br />83-128 <br />3 <br />30 <br />97 <br />101 <br />73-136 <br />4 <br />30 <br />95 <br />98 <br />83-127 <br />3 <br />30 <br />93 <br />95 <br />78-120 <br />2 <br />30 <br />97 <br />102 <br />82-129_ <br />5 <br />30 <br />97 <br />103 <br />82-130 <br />5 <br />30 <br />Surrogate Quality Control <br />.1 <br />Batch number: 0413SAOBA <br />Trifluorotoluene-F <br />+ <br />4272159 119 <br />Blank 105 <br />LCS 111 <br />111 <br />MS <br />MS 109 <br />Limits; 57-146 <br />Analysis Name: TPH-GRO - Waters <br />Batch number: 0413SA08B <br />Trifluorotoluene-F <br />4272160 120 <br />4272161 130 <br />4272162 137 <br />ri <br />*- Outside of specification l <br />() ) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />