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Lancaster <br />Laboratories <br />Quality Control Summary <br />Client Name: ChevronTexaca <br />Reported: 12/05/03 at 08:00 AM Group Number: 875291 <br />Laboratory Compliance Quality Control <br />B1 <br />Aaalysis Name <br />Batch number. 03323AOSB <br />TPH-GRO - Waters <br />Batch number: 03323A16A <br />TPH-GRo - Waters <br />Batch number: 033240027A <br />Methanol (by Direct Injection) <br />Batch number: P033233AA <br />Ethanol <br />Methyl Tertiary Butyl Ether <br />di -Isopropyl ether <br />Sample Matrix Quality Control <br />HS MD MS/MSD RPD BKO <br />%R8c %RSC Limits RPD MAX Conc <br />Sample number(s); 4166554-4166556 <br />101 101 63-154 0 30 <br />Sample number(s): 4166557 <br />103 63-154 <br />Sample number(s): 4166554-4166557 <br />112 65* 73-117 52* 20 <br />Sample number(s): 4166554-4166558 <br />96 96 38-149 0 30 <br />96 97 69-134 1 30 <br />89 89 75-130 0 30 <br />*-Outside of specification <br />(1) The result for one or bath determinations was less than five times the LOQ. <br />(oQ) The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />MEEMBIER <br />2425 New Holland Pike <br />Po Box 72425 <br />Lancaster, PA 17605-2.425 <br />717-656-2300 <br />Fax: 717-656-2681 <br />4 <br />DUP DVP <br />Conc RPD <br />Page I of 3 <br />RPD RPD Max <br />30 <br />DuP <br />RPD <br />Max <br />2216 Rev. 3110/03 <br />Analysis Name <br />ank <br />Result <br />Blank <br />Report <br />LCS <br />LCSD LCS/LCSD <br />Batch <br />MDL <br />Units <br />%REC <br />$REC Limits <br />number: 03323AO8B <br />TPH-GRO - Waters <br />Sample <br />number(s): <br />4166554-4166556 <br />N.D. <br />50. <br />ug/l <br />118 <br />Batch number: 03323A16A <br />TPH-GRO <br />Sample <br />number(s): <br />4166557 <br />70-130 <br />f <br />- Waters <br />N.D. <br />50, <br />ug/1 <br />107 <br />103 70-130 <br />Batch number: 033240027A <br />Methanol (by Direct Injection) <br />Sample <br />number(s): <br />4166554-4166557 <br />N.D. <br />200. <br />u9/1 <br />108 <br />Batch number: P033233AA <br />78-114 <br />Ethanol <br />Sample <br />number(s): <br />4166554-4166558 <br />Methyl Tertiary Butyl Ether <br />N D <br />N.D. <br />N.D. <br />so. <br />ug/l <br />96 <br />46-145 <br />di ether <br />N D, <br />0.5 <br />ug/l <br />96 <br />77-127 <br />Ethyl t -butyl ether <br />N.D. <br />0'5 <br />ug/1 <br />74-125 <br />t -Amyl methyl ether <br />N.D. <br />0.5 <br />ug/1 <br />987 2 <br />92 <br />74_120 <br />t -Butyl alcohol <br />N.D. <br />0.5 <br />ug/l <br />98 <br />79-113 <br />enzene <br />�,2-Dichloroethane <br />N.D. <br />S. <br />0.5 <br />ug/l <br />91 <br />53-147 <br />ug/l <br />100 <br />85-117 <br />'7!"o1uene015 <br />N.D, <br />N.D. <br />ug/l <br />94 <br />77-132 <br />1,2-Dibromoethane <br />N.D,U <br />0'5 <br />ug/l <br />97 <br />85-115 <br />Ethylbenzene <br />N.D. <br />'S <br />u9/1 <br />95 <br />81-114 <br />r <br />Xylene (Total) <br />N.D. <br />0'5 <br />ug/1 <br />95 <br />62-119 <br />0.5 <br />ug/I <br />99 <br />84-120 <br />Aaalysis Name <br />Batch number. 03323AOSB <br />TPH-GRO - Waters <br />Batch number: 03323A16A <br />TPH-GRo - Waters <br />Batch number: 033240027A <br />Methanol (by Direct Injection) <br />Batch number: P033233AA <br />Ethanol <br />Methyl Tertiary Butyl Ether <br />di -Isopropyl ether <br />Sample Matrix Quality Control <br />HS MD MS/MSD RPD BKO <br />%R8c %RSC Limits RPD MAX Conc <br />Sample number(s); 4166554-4166556 <br />101 101 63-154 0 30 <br />Sample number(s): 4166557 <br />103 63-154 <br />Sample number(s): 4166554-4166557 <br />112 65* 73-117 52* 20 <br />Sample number(s): 4166554-4166558 <br />96 96 38-149 0 30 <br />96 97 69-134 1 30 <br />89 89 75-130 0 30 <br />*-Outside of specification <br />(1) The result for one or bath determinations was less than five times the LOQ. <br />(oQ) The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />MEEMBIER <br />2425 New Holland Pike <br />Po Box 72425 <br />Lancaster, PA 17605-2.425 <br />717-656-2300 <br />Fax: 717-656-2681 <br />4 <br />DUP DVP <br />Conc RPD <br />Page I of 3 <br />RPD RPD Max <br />30 <br />DuP <br />RPD <br />Max <br />2216 Rev. 3110/03 <br />