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Lancaster <br />Laboratories <br />Quality Control Summary <br />Client Name: ChevronTexaco Group Number: 875291 <br />Reported: 12/05/03 at 08:00 AM <br />Surrogate Quality Control <br />4166554 116 <br />4166555 103 <br />4166556 87 <br />4166557 95 <br />Blank 115 <br />LCS 115 <br />MS 117 <br />MSD 88 <br />Limits: 72-128 <br />Analysis Name: BTEX+5 Oxygenates+EDC+EDB+ETON <br />Batch number: P033233AA <br />Dibromofluoromethane 1,2-Dichloroethane-c14 <br />Toluene -d8 <br />100 <br />98 <br />99 <br />98 <br />98 <br />99 <br />98 <br />98 <br />98 <br />85-112 <br />*- Outside of specification <br />{1) The result for one or both determinations was less than five times the LOQ. <br />I The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />M E M B E R 2425 New Holland Pike <br />Box 12425 <br />La <br />� Lancaster, PA 17605-2425 <br />717-656-2300 fax: 717-656-2681 <br />Page 3 of 3 <br />4-Bromo£luorobenzene <br />88 <br />86 <br />86 <br />87 <br />92 <br />88 <br />89 <br />89 <br />89 <br />83-113 <br />2216 Rev. 3/10/03 <br />4166554 <br />97 <br />90 <br />4166555 <br />96 <br />89 <br />4166556 <br />97 <br />90 <br />4166557 <br />97 <br />90 <br />4166558 <br />96 <br />B9 <br />Blank <br />98 <br />89 <br />�--LCs <br />97 <br />89 <br />- ... <br />MS <br />97 <br />90 <br />MSD <br />98 <br />89 <br />Limits: <br />81-120 <br />82-112 <br />r' <br />! k <br />Toluene -d8 <br />100 <br />98 <br />99 <br />98 <br />98 <br />99 <br />98 <br />98 <br />98 <br />85-112 <br />*- Outside of specification <br />{1) The result for one or both determinations was less than five times the LOQ. <br />I The background result was more than four times the spike added. <br />Lancaster Laboratories, Inc. <br />M E M B E R 2425 New Holland Pike <br />Box 12425 <br />La <br />� Lancaster, PA 17605-2425 <br />717-656-2300 fax: 717-656-2681 <br />Page 3 of 3 <br />4-Bromo£luorobenzene <br />88 <br />86 <br />86 <br />87 <br />92 <br />88 <br />89 <br />89 <br />89 <br />83-113 <br />2216 Rev. 3/10/03 <br />