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Lancaster <br />Laboratories Analysis Report' -4 <br />2425 New Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 •717-656-2300 Fax �717-656-2681 - W WW.Iancasterlat)s.com n <br />Quality Control Summary <br />Client Name: ChevronTexaco <br />number(s): 4266187 <br />41-155 <br />13 <br />Reported: 05/14/04 at <br />03:46 PM <br />9 <br />Group Number: <br />894513 <br />95 83-128 <br />Laboratory Compliance Quality <br />Control <br />ARAlvain Name <br />Blank <br />Blank Report <br />LCS LCSD <br />LCS/LCSD <br />Methyl Tertiary Butyl Ether <br />ReSUlt <br />N.D. <br />IDSL Units <br />0.5 ug/l <br />REC IRE c <br />97 <br />Limits <br />di -Isopropyl ether <br />N.D. <br />0.5 ug/l <br />93 <br />77-127 <br />Ethyl t -butyl ether <br />N.D. <br />0.5 ug/l <br />91 <br />67-130 <br />t -Amyl methyl ether <br />N.D. <br />0.5 ug/1 <br />96 <br />74-120 <br />79-113 <br />t -Butyl alcohol <br />Benzene <br />N.D. <br />5. ug/1 <br />99 <br />57-141 <br />1,2-Dichloroethane <br />N.D. <br />N.D. <br />0,5 ug/l <br />0.5 ug/1 <br />98 <br />91 <br />85-117 <br />Toluene <br />1,2-Dibromoethane <br />N.D. <br />0,5 u9/1 <br />95 <br />77-132 <br />85-115 <br />Ethylbenzene <br />N.A. <br />N.D. <br />0.5 ug/l <br />95 <br />e1-114 <br />Xylene (Total) <br />N. 1). <br />0.5 ug/l <br />0.5 ug/l <br />94 <br />97 <br />82-119 <br />84-120 <br />Sample Matrix <br />Quality Control <br />Aualvais„Name <br />MS <br />REC <br />MSD MS/MSD RPD BRG <br />N&KCimits <br />�- BEP XAX cone <br />DUP <br />Conc <br />Batch number: 04126A07A <br />Sample <br />number(a); 4266187 <br />TPH-GRO - Waters <br />105 <br />63-154 <br />Batch number: 04126A55A <br />Sample <br />number(s): 4266196-4266214 <br />TPH-GRO - Waters <br />93 <br />63-154 <br />Batch number: 04127A07D <br />Sample <br />number(s): 4266188-4266192 <br />TPH-GRO - Waters <br />89 <br />63-154 <br />Batch number: 04127A07E <br />Sample <br />number(s): 4266193-4266195 <br />TPR-GRO - Waters <br />89 <br />63-154 <br />Batch number: 041280016A <br />Methanol (by Direct injection) <br />Batch number: 041290017A <br />Methanol (by Direct Injection) <br />Batch number: 041310024A <br />Methanol (by Direct Injection) <br />Batch number: P041282AA <br />Methyl Tertiary Butyl Ether <br />Benzene <br />Toluene <br />Ethylbenzene <br />Xylene (Total) <br />Batch number: P041311AA <br />Ethanol <br />Methyl Tertiary Butyl Ether <br />di -Isopropyl ether <br />Ethyl t -butyl ether <br />t -Amyl methyl ether <br />t -Butyl alcohol <br />Benzene <br />Sample number(s): 4266188 <br />92 92 72-122 0 20 <br />Sample number(s): 4266169-4266208 <br />92 92 72-122 0 20 <br />Sample number(s); 4266209-4266214 <br />96 96 72-122 0 20 <br />Sample <br />number(s): 4266187 <br />41-155 <br />13 <br />101 <br />93 69-134 <br />9 <br />30 <br />106 <br />95 83-128 <br />11 <br />30 <br />103 <br />93_ 83-127 <br />10 <br />30 <br />104 <br />93 62-3.29 <br />11 <br />30 <br />104 <br />94 82-130 <br />11 <br />30 <br />Sample number(s): 4266188-4266195,426(;197-4266203 <br />82 <br />72 <br />41-155 <br />13 <br />30 <br />93 <br />89 <br />69-134 <br />1 <br />30 <br />92 <br />87 <br />75-130 <br />5 <br />30 <br />91 <br />88 <br />78-119 <br />4 <br />30 <br />98 <br />90 <br />77-117 <br />8 <br />30 <br />140 <br />128 <br />51-147 <br />8 <br />30 <br />98 <br />94 <br />83-128 <br />1 <br />30 <br />*- Outside of specification <br />0 ) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />Page 2 of 6 <br />i <br />RPD RPD Max <br />DUP Dup RPD <br />RED max <br />IN <br />I� I <br />X71 <br />r <br />