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F, <br />Lancaster <br />Laboratories analysis Report <br />! 2425 New Holland Pike, PO Box 12425, Lancasler, PA 1 7 605-242 5 •717-656-2300 Fax. 717-656-2681 • W W W.laMa$tetiabs.com <br />r— <br />Quality Control Summary <br />Client Name: ChevronTexaCo Group Numher: 894513 <br />Reported: 05/14/04 at 43:46 PM <br />I: Surrogate Quality Control <br />104 <br />105 <br />104 <br />101 <br />103 <br />102 <br />106 <br />103 <br />103 <br />104 <br />105 <br />105 <br />106 <br />105 <br />104 <br />102 <br />104 <br />102 <br />103 <br />102 <br />102 <br />99 ' <br />104 <br />104 <br />Limits: 80-132 <br />Analysis Name: Methanol and Ethanol <br />Batch number: 041310024A <br />- '- Acetone <br />*- Outside of specification <br />k _ (1) The result for one or both determinations was less than five tunes the LOQ. <br />(--V2)- The background result was more than four times the spike added. <br />Page 5 of 6 <br />4-Bromofluorobenzene <br />93 <br />95 <br />94 <br />95 <br />4266210 <br />93 <br />4266211 <br />4266212 <br />93 <br />97 <br />4266213 <br />95 <br />1 <br />4266214 <br />98 <br />j <br />Blank <br />94 <br />Toluene -d8 <br />LCS <br />94 <br />97 <br />Ms <br />95 <br />Blank 101 <br />MSL <br />94 <br />*- Outside of specification <br />k _ (1) The result for one or both determinations was less than five tunes the LOQ. <br />(--V2)- The background result was more than four times the spike added. <br />Page 5 of 6 <br />4-Bromofluorobenzene <br />93 <br />95 <br />94 <br />95 <br />LilnlLtl: CV -1 J4 <br />Analysis Name: BTEX+MTBE by 8260B <br />Batch number: P041282AA <br />j <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4266187 103 <br />97 <br />95 <br />Blank 101 <br />97 <br />94 <br />LCS 103 <br />98 <br />95 <br />MS 103 <br />97 <br />95 <br />MSB 100 <br />98 <br />94 <br />Limits: 81-120 <br />62-112 <br />85-112 <br />g <br />Analysis Name: STEX+5 Oxygenate s+EDC+EDB+ETOH <br />i <br />Batch number: P041311AA <br />*- Outside of specification <br />k _ (1) The result for one or both determinations was less than five tunes the LOQ. <br />(--V2)- The background result was more than four times the spike added. <br />Page 5 of 6 <br />4-Bromofluorobenzene <br />93 <br />95 <br />94 <br />95 <br />