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1 Lancaster <br />Laboratories <br />Surrogate Quality Control <br />Analysis Name TPH-GRO - Waters <br />Batch number 03008A07E <br />■ Trifluorotoluene-F <br />3975445 91 <br />3975446 89 <br />3975447 89 <br />'3975448 89 <br />3975449 88 <br />Blank 89 <br />LCS 108 <br />'LCSD 107 <br />MS 288* <br />Limits 57-146 <br />Analysis Name Methanol and Ethanol <br />Batch number 030130006A <br />Acetone <br />' *- Outside of specification <br />The result for one or both detertnmations was less than five times the LOQ <br />e background result was more than four times the spike added <br />Lancaster Laboratories Inc <br />' M B F- R 2425 New Holland Pike <br />® Box 9 <br />Lancaster, <br />PA PA 17605 2425 <br />717-656 2300 fax 717 656 2681 <br />Page 3 of 5 <br />DUP Dup <br />RPD <br />RPD Max <br />?710; Rnv inIM7 <br />Quality <br />Control Summary <br />I <br />Client Name ChevronTexaco <br />Group Number 837261 <br />Reported 01/23/03 <br />at 02 23 PM <br />' <br />Sample <br />Matrix <br />Quality Control <br />MS <br />MSD <br />MS/MSD <br />RPD BXG DUP <br />sis Name <br />%REC <br />%REC <br />Limits <br />RPD <br />MAX Conc Conc <br />'Anal <br />Xylene (Total) <br />113 <br />113 <br />82-130 <br />0 <br />30 <br />Batch number N030102AC <br />Sample <br />number(s) <br />3975449 <br />Methyl t -butyl ether <br />103 <br />104 <br />69-134 <br />1 <br />30 <br />Benzene <br />114 <br />115 <br />78-134 <br />1 <br />30 <br />Toluene <br />114 <br />112 <br />83-127 <br />2 <br />30 <br />Ethylbenzene <br />112 <br />113 <br />82-134 <br />1 <br />30 <br />Xylene (Total) <br />113 <br />113 <br />82-130 <br />0 <br />30 <br />Batch number N030121AA <br />Sample <br />number(s) 3975447 <br />Ethanol <br />116 <br />115 <br />34-163 <br />0 <br />30 <br />Methyl t -butyl ether <br />101 <br />101 <br />69-134 <br />0 <br />30 <br />dx-Isopropyl ether <br />106 <br />105 <br />68-133 <br />0 <br />30 <br />Ethyl t -butyl ether <br />96 <br />99 <br />73-123 <br />2 <br />30 <br />t -Amyl methyl ether <br />96 <br />97 <br />69-118 <br />1 <br />30 <br />t -Butyl alcohol <br />108 <br />108 <br />51-148 <br />1 <br />30 <br />118 <br />11 <br />78-134 <br />2 <br />30 <br />Dichloroethane <br />118 <br />1155 <br />73-136 <br />3 <br />30 <br />1#ene <br />ene <br />114 <br />112 <br />83-127 <br />1 <br />30 <br />1,2-Dibromoethane <br />105 <br />105 <br />78-120 <br />0 <br />30 <br />Ethylbenzene <br />113 <br />112 <br />82-134 <br />1 <br />30 <br />' <br />Xylene (Total) <br />115 <br />113 <br />82-130 <br />2 <br />30 <br />Surrogate Quality Control <br />Analysis Name TPH-GRO - Waters <br />Batch number 03008A07E <br />■ Trifluorotoluene-F <br />3975445 91 <br />3975446 89 <br />3975447 89 <br />'3975448 89 <br />3975449 88 <br />Blank 89 <br />LCS 108 <br />'LCSD 107 <br />MS 288* <br />Limits 57-146 <br />Analysis Name Methanol and Ethanol <br />Batch number 030130006A <br />Acetone <br />' *- Outside of specification <br />The result for one or both detertnmations was less than five times the LOQ <br />e background result was more than four times the spike added <br />Lancaster Laboratories Inc <br />' M B F- R 2425 New Holland Pike <br />® Box 9 <br />Lancaster, <br />PA PA 17605 2425 <br />717-656 2300 fax 717 656 2681 <br />Page 3 of 5 <br />DUP Dup <br />RPD <br />RPD Max <br />?710; Rnv inIM7 <br />