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Lancaster <br />Laboratories <br />1 <br />Quality Control Summary <br />' Client Name ChevronTexaco Group Number 840483 <br />Reported 02/20/03 at 02 30 PM <br />Sample Matrix Quality Control <br />' MS MSD MS/MSA APD BK(; DUP <br />Analysis N <br />'Batch number P030441AA <br />Methyl Tertiary Butyl Ether <br />Benzene <br />Toluene <br />Ethylbenzene <br />' Xylene (Total) <br />' Analysis Name TPH-GRO - waters <br />Batch number 03037A55A <br />Trifluorotoluene-F <br />%REC <br />IRSC Limits <br />RPD <br />NM COnc <br />Sample <br />number(S) 3990508 <br />112 <br />113 69-134 <br />1 <br />30 <br />110 <br />111 83-128 <br />1 <br />30 <br />103 <br />103 83-127 <br />0 <br />30 <br />105 <br />104 82-134 <br />1 <br />30 <br />107 <br />105 82-130 <br />2 <br />30 <br />3990504 99 <br />3990505 102 <br />3990506 109 <br />3990507 100 <br />' <br />CSD <br />100 <br />S 107 <br />CSD 104 <br />MS 105 <br />'Limits 57-146 <br />Analysis Name Methanol and Ethanol <br />Batch number 030430017A <br />Acetone <br />Surrogate Quality Control <br />Cone <br />Page 2 of 3 <br />DUFF <br />Dup <br />RPD <br />Max <br />Outside of specification <br />The result for one or both determinations was less than five times the LOQ <br />- The background result was more than four times the spike added <br />3990504 99 <br />' M E M H E R <br />®Po <br />2425 New Holland Pike <br />Box 12425 <br />Lancaster PA 17605-2425 <br />3990505 101 <br />3990506 102 <br />3990507 101 <br />Blank 99 <br />LCS 97 <br />' <br />MS 97 <br />MSD 98 <br />Llmlt6 72-128 <br />'Analysis Name BTEX + Oxygenates by <br />826013 <br />Batch number P030401AA <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -de <br />4-Bromofluorobenzene <br />100 <br />99 <br />102 <br />96 <br />'3990504 <br />3990505 100 <br />101 <br />100 <br />95 <br />3990506 101 <br />101 <br />100 <br />95 <br />3990507 100 <br />99 <br />101 <br />96 <br />Blank 102 <br />102 <br />101 <br />95 <br />LCS 102 <br />1.01 <br />102 <br />97 <br />MS 101 <br />97 <br />102 <br />100 <br />MSD 100 <br />104 <br />102 <br />103 <br />Outside of specification <br />The result for one or both determinations was less than five times the LOQ <br />- The background result was more than four times the spike added <br />2216 Rev 1012102 <br />Lancaster Laboratories, Inc <br />' M E M H E R <br />®Po <br />2425 New Holland Pike <br />Box 12425 <br />Lancaster PA 17605-2425 <br />717-656-2300 Fax 717-656-2681 <br />2216 Rev 1012102 <br />