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Lancaster <br />� Laboratories <br />1 <br />Quality Control Summary <br />Client Name ChevronTexaco Group Number 842369 <br />Reported 03/10/03 at 09 30 AM <br />� I <br />I <br />Analysis Name TPH-GRO - Waters <br />Batch number 03056A07B <br />Trifluorotoluene-F <br />� I <br />Limits 57-146 <br />Analysis Name TPH-GRO - waters <br />Batch number 030S6AO7C <br />Trifluorotoluene-F <br />Surrogate Quality Control <br />Page 2 of 3 <br />'4000234 <br />4000238 <br />89 <br />87 <br />LCS <br />111, <br />10 104 <br />'Blank <br />LCSD <br />124 <br />86 <br />MS <br />129 <br />SD <br />MSD <br />132 <br />� I <br />Limits 57-146 <br />Analysis Name TPH-GRO - waters <br />Batch number 030S6AO7C <br />Trifluorotoluene-F <br />Surrogate Quality Control <br />Page 2 of 3 <br />'4000234 <br />87 <br />4000235 <br />87 <br />4000236 <br />88 <br />00237 <br />87 <br />86 <br />'nk <br />109 <br />SD <br />124 <br />MS <br />129 <br />MSD <br />132 <br />' <br />Lancaster Laboratories Inc <br />M E M B E R <br />2425 New Holland Pike <br />®PO <br />1 <br />Limits 57-146 <br />717-656-2300 Fax 717-656-21581 <br />Analysis Name Methanol and Ethanol <br />Batch number 030570020A <br />'Acetone <br />4000234 99 <br />4000235 103 <br />4000236 102 <br />4000237 101 <br />1 <br />4000238 101 <br />Blank 104 <br />LCS 101 <br />MS 103 <br />102 <br />'MSD <br />Limits 72-128 <br />Analysis Name BTEX + Oxygenates by <br />8260B <br />Batch number N030601AA <br />1 <br />Dibromo€luoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />4000234 104 <br />101 <br />106 <br />100 <br />4000235 103 <br />101 <br />107 <br />101 <br />105 <br />101 <br />106 <br />100 <br />'4000236 <br />4000237 103 <br />103 <br />108 <br />101 <br />4000238 103 <br />101 <br />106 <br />99 <br />Blank 101 <br />100 <br />107 <br />100 <br />1 *- Outside of specification <br />The result for one or both determinations was less than five times the LOQ <br />The background result was more than four times the spike added <br />2216 Rev 10/2102 <br />Lancaster Laboratories Inc <br />M E M B E R <br />2425 New Holland Pike <br />®PO <br />1 <br />Box 12425 <br />Lancaster PA 17605-2425 <br />717-656-2300 Fax 717-656-21581 <br />2216 Rev 10/2102 <br />