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Lancaster <br />• Laboratories <br />Page 3 of 3 <br />Quality Control Summary <br />Client Name ChevronTexaco Group Number 840483 <br />Reported 02/20/03 at 02 30 PM <br />Surrogate Quality Control <br />Limits 86-116 80-120 88-110 86-115 <br />Analysis Name BTEX + Oxygenates by 82608 <br />Batch number P030441AA <br />Dibromofluoromethane 1,2-D3.chloroethane-d4 Toluene -d8 4-Bromofluorobenzene <br />3990508 <br />100 <br />101 <br />101 <br />96 <br />Blank <br />102 <br />100 <br />100 <br />95 <br />LCS <br />102 <br />107 <br />100 <br />97 <br />LCSD <br />103 <br />102 <br />102 <br />98 <br />Ms <br />103 <br />98 <br />101 <br />98 <br />MSD <br />103 <br />105 <br />101 <br />97 <br />Limits <br />86-118 <br />80-120 <br />88-110 <br />86-115 <br />• <br />*- Outside of specification <br />The result for one or both determinations was less than five times the LOQ <br />The background result was more than four times the spike added <br />Lancaster Laboratories Inc <br />MEMBER 2425 New Holland Pike <br />PO Box 12425 <br />Lancaster, PA 17605-2425 <br />717-656-2300 Fax 717 656 2681 2216 Rev 1012/02 <br />