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0 <br />Lancaster <br />Laboratories <br />Analysis Report <br />2425 NOW HoAaixd piks PO Boot 12425 tanoastel, PA 17605 2425.7j7 656 23N Fax 717-658.2681 • WWW iancastarlab6 com <br />Quality Control Summary <br />w_ Outside of specification <br />(1) The result for one or both determinations was less than five tittles the LUQ <br />�(2) The background result was more than four tines the spike added <br />Page ] of 3 <br />RPD RPD Max <br />1 30 <br />1 30 <br />DUP <br />RPD <br />Dug <br />RFD <br />Max <br />Client Name ChevronTexaco <br />Group Number <br />842369 <br />Reported 03/10/03 at 09 <br />30 AM <br />Laboratory Compliance Quality <br />Control <br />Blank <br />Blank Report LCS <br />LCSD <br />LCS/LCSD <br />Analysis Name <br />Result <br />MDL Units %R$C <br />%REC <br />Limits <br />Batch number 03056A07B <br />Sample <br />number(s) 4000238 <br />TPH-GRO - Waters <br />N D <br />50 ug/l 110 <br />11.2 <br />70-130 <br />Batch number 03056A07C <br />Sample <br />number($) 4000234-4000237 <br />TPH-GRO Waters <br />N D <br />50 u9/1 110 <br />112 <br />70-130 <br />Batch number 030570020A <br />Sample <br />number(s) 4000234-4000238 <br />Methanol (by Direct in)ection) <br />N D <br />200 u9/1 92 <br />64-130 <br />Batch number N030601AA <br />Sample <br />number(s) 4000234-4000238 <br />Ethanol <br />N D <br />50 ug/1 100 <br />43-159 <br />Methyl Tertiary Butyl Ether <br />N D <br />5 ug/l 100 <br />77-127 <br />di -Isopropyl ether <br />N D <br />5 ug/l 96 <br />74-125 <br />Ethyl t -butyl ether <br />N D <br />5 u9/1 97 <br />74-120 <br />t -Amyl methyl ether <br />N D <br />5 u9/1 96 <br />79-113 <br />t -Butyl alcohol <br />N D <br />5 ug/l BO <br />53-147 <br />Benzene <br />N D <br />5 ug/l 101 <br />85-117 <br />1,2-Dichloroethane <br />N D <br />5 ug/l 99 <br />77-132 <br />Toluene <br />N D <br />5 ug/l 101 <br />85-115 <br />1,2-Dibromoethane <br />N D <br />5 ug/l 98 <br />81-114 <br />Ethylbenzene <br />N D <br />5 ug/l 101 <br />82-119 <br />. <br />Xylene (Total) <br />N D <br />5 ug/l 103 <br />84-120 <br />Sample Matrix Quality <br />Control <br />US <br />MSD DSS/MSI) RPD <br />BKG <br />DBP <br />Analysis Name <br />JILEC <br />vaREC Limits RPD MAX <br />Conc <br />conc <br />Batch number 03056A07B <br />Sample <br />numbers) 4000238 <br />TPH-GRO - Waters <br />111 <br />124 70-130 8 30 <br />Batch number 05056A07C <br />Sample <br />number (s) 4000234-4000237 <br />TPH-GRO - Waters <br />111 <br />124 70-130 8 30 <br />Batch number 030570020A <br />Sample <br />number(s) 4000234-4000238 <br />Methanol (by Direct Inaection) <br />92 <br />92 69-127 0 20 <br />Batch number N030601AA <br />Sample <br />number(a) 4000234-4000238 <br />Ethanol <br />100 <br />102 34-163 2 30 <br />Methyl Tertiary Hutyl Ether <br />99 <br />101 69-134 2 30 <br />di -Isopropyl ether <br />97 <br />100 75-130 3 30 <br />Ethyl t -butyl ether <br />97 <br />100 73-123 4 30 <br />t -Amyl methyl ether <br />96 <br />97 77-117 2 30 <br />t -Butyl alcohol <br />83 <br />84 39-155 2 30 <br />Benzene <br />104 <br />107 83-128 2 30 <br />1,2-DLchloroethane <br />103 <br />104 73-136 1 30 <br />Toluene <br />105 <br />107 83-127 2 30 <br />1,2-Dibromoethane <br />100 <br />101 78-120 1 30 <br />Ethylbenzene <br />107 <br />108 82-134 1 30 <br />Xylene (Total) <br />108 <br />110 82-130 2 30 <br />w_ Outside of specification <br />(1) The result for one or both determinations was less than five tittles the LUQ <br />�(2) The background result was more than four tines the spike added <br />Page ] of 3 <br />RPD RPD Max <br />1 30 <br />1 30 <br />DUP <br />RPD <br />Dug <br />RFD <br />Max <br />