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Lancaster Laboratories REPRINT <br />M *yWa -Q*rxo1 summary <br />Client Name: ChevzonTexaco Group Number: 815748 <br />Reported: 08/08/02 at 06:09 PM <br />Surrogate Quality Control <br />Batch number: 022050005A <br />Acetone <br />3858362 101 <br />Blank 100 <br />LCs 99 <br />MS 100 <br />MSD 103 <br />Limits: 72-128 <br />Analysis Name: BTEX + Oxygenates by 82608 <br />Batch number: N022101AA <br />Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene -d8 <br />Page 2 of 2 <br />4-Bromofluorobenzene <br />3858362 <br />109 <br />95 <br />99 <br />99 <br />3858363 <br />109 <br />95 <br />99 <br />97 <br />Blank <br />107 <br />95 <br />99 <br />98 <br />LCS <br />105 <br />94 <br />101 <br />105 <br />Ms <br />105 <br />94 <br />101 <br />106 <br />MSD <br />105 <br />96 <br />102 <br />105 <br />Limits: <br />0 <br />86-118 <br />80-120 <br />88-110 <br />*- Outside of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />The background result was more than four times the spike added. <br />—0 <br />Lancaster Laboratories, Inc. <br />M E M 13 E R 2425 New Holland Pike <br />PO Box 12425 <br />Lanca <br />425 <br />® 717-65-2ter, 00 1Fax:7 7-6 <br />717-65b-2300 Fax: 717-65b-2681 <br />86-115 <br />2216 Rev- 9111100 <br />