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Lancaster Laboratories <br />Where quality is a science. <br />Lancaster Laboratories Sample No. WW 3869019 <br />Collected:07/28/2002 00:00 <br />through 07/30/2002 00:00 <br />Submitted: 08/01/2002 09:40 <br />Reported: 08/15/2002 at 15:38 <br />Discard: 09/15/2002 <br />QA -T-0207282930 NA Water <br />Facility# 95775 Job# 386408 GRD <br />301 W Kettleman-Lodi T0607700839 QA <br />WKLQA <br />Page 1 of 1 <br />Account Number: 10906 <br />ChevronTexaco <br />6001 Bollinger Canyon Rd L4310 <br />San Ramon CA 94583 <br />State of California Lab Certification No. 2116 <br />CAT <br />No. Analysis Name <br />01728 TPH-GRO - Waters <br />01594 BTEX + Oxygenates by 8260B <br />01146 GC VOA Water Prep <br />01163 GC/MS VOA Water Prep <br />Laboratory Chronicle <br />Dilution <br />Analysis <br />Method <br />As Received <br />Date and Time <br />N. CA LUFT Gasoline <br />CAT <br />08/01/2002 23:27 <br />Method <br />As Received <br />Method <br />SW -846 8260B <br />Dilution <br />No. <br />Analysis Name <br />CAS Number <br />Result <br />Detection <br />Units <br />Factor <br />Limit <br />01728 <br />TPH-GRO - Waters <br />n.a. <br />N.D. <br />50. <br />ug/l <br />1 <br />The reported concentration of <br />TPH-GRO does not <br />include MTBE or <br />other <br />gasoline constituents eluting <br />prior to the C6 <br />(n -hexane) TPH-GRO range <br />start time. <br />A site-specific MSD sample was <br />not submitted for <br />the project. A LCS/LCSD <br />0 <br />was performed to demonstrate precision and accuracy at a batch <br />level. <br />01594 <br />BTEX + Oxygenates by 8260E <br />02010 <br />Methyl t -butyl ether <br />1634-04-4 <br />N -D. <br />2. <br />ug/l <br />1 <br />05401 <br />Benzene <br />71-43-2 <br />N.D. <br />0.5 <br />ug/l <br />1 <br />05407 <br />Toluene <br />108-68-3 <br />N.D. <br />0.5 <br />ug/1 <br />1 <br />05415 <br />Ethylbenzene <br />100-41-4 <br />N.D. <br />0.5 <br />ug/1 <br />1 <br />06310 <br />Xylene (Total) <br />1330-20-7 <br />N.D. <br />0.5 <br />ug/l <br />1 <br />State of California Lab Certification No. 2116 <br />CAT <br />No. Analysis Name <br />01728 TPH-GRO - Waters <br />01594 BTEX + Oxygenates by 8260B <br />01146 GC VOA Water Prep <br />01163 GC/MS VOA Water Prep <br />Laboratory Chronicle <br />#=Laboratory MethodDetectiQn L' itLe t�a�et detection limit <br />8 va'R Abe er La oda- e� s, n . <br />N.D.=Not det t t r vct <br />PO Box 12425 <br />WIN Lancaster, PA 17605-2425 <br />717-656-2300 Fax: 717-656-2681 <br />Dilution <br />Analysis <br />Method <br />Trial# <br />Date and Time <br />N. CA LUFT Gasoline <br />1 <br />08/01/2002 23:27 <br />Method <br />Nicole.S Lamoreaux <br />n.a. <br />SW -846 8260B <br />1 <br />08/02/2002 19:36 <br />SW -846 5030B <br />1 <br />08/01/2002 23:27 <br />SW -846 5030E <br />1 <br />08/02/2002 19:36 <br />#=Laboratory MethodDetectiQn L' itLe t�a�et detection limit <br />8 va'R Abe er La oda- e� s, n . <br />N.D.=Not det t t r vct <br />PO Box 12425 <br />WIN Lancaster, PA 17605-2425 <br />717-656-2300 Fax: 717-656-2681 <br />2216 Rev. 9/11/00 <br />Dilution <br />Analyst <br />Factor <br />Melissa D Mann <br />1 <br />Nicole S Lamoreaux <br />1 <br />Melissa D Mann <br />n.a. <br />Nicole.S Lamoreaux <br />n.a. <br />2216 Rev. 9/11/00 <br />