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Report Number: 25772 XANEALY7YCAL Date : 4/4/2002 LLC Project Name: Chevron 9-57751301 W. Kettleman Lane, Lodi, Ca. Project Number: 77CH.43452.00.0550 Sample : Mld#2 Matrix: Water Lab Number : 25772-03 Sample Date A/312002 TPH as Gasoline Toluene - d8 (Surr) 4-Bromofluorobenzene (Surr) < 50 50 ug/L EPA 8260B 4/4/2002 104 % Recovery EPA 8260B 4/4/2002 96.9 % Recovery EPA 82606 4/4/2002 Approved By: J I Kiff 720 Olive Drive, Suite D Davis, CA 95616 530-297-4 0 Method Measured Reporting Analysis Date Parameter Value Limit Units Method Analyzed Benzene < 0.50 0.50 ug/L EPA 82608 4/4/2002 Toluene < 0.50 0.50 ug/L EPA 82608 4/4/2002 Ethylbenzene < 0.50 0.50 ug/L EPA 8260B 4/4/2002 Total Xylenes < 0.50 0.50 ug/L EPA 8260B 4/4/2002 Methyl -t -butyl ether (MTBE) < 0.50 0.50 ug/L EPA 82608 4/4/2002 Dilsopropyl ether (DIPS) -40.50 0.50 ug/L EPA 8260B 4/4/2002 Ethyl -t -butyl ether (ETRE) 40.50 0.50 ug/L EPA 8260B 4/4/2002 Tert-amyl methyl ether (TAME) < 0.50 0.50 ug/L EPA 8260B 4/4/2002 Tort -Butanol < 5.0 5.0 ug/L EPA 8260B 4/4/2002 Methanol <50 50 ug/L EPA 8260B 4/4/2002 anol < 5.0 5.0 ug/L EPA 8260B 414/2002 W-Dichloroethane < 0.50 0.50 ug/L EPA 82606 4/4/2002 1,2-Dlbromoethane < 0.50 0.50 ug/L EPA 82608 4/4/2002 TPH as Gasoline Toluene - d8 (Surr) 4-Bromofluorobenzene (Surr) < 50 50 ug/L EPA 8260B 4/4/2002 104 % Recovery EPA 8260B 4/4/2002 96.9 % Recovery EPA 82606 4/4/2002 Approved By: J I Kiff 720 Olive Drive, Suite D Davis, CA 95616 530-297-4 0