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Sequoia <br />� Analytical <br />1551 industrial Road <br />San Carfos CA 94070-4111 <br />(650) 232-9600 <br />FAX (650) 2.32-9612 <br />Blaine Tech Services <br />Project <br />Chevron(3) <br />Sampled <br />6121199 <br />1680 Rogers Avenue <br />Project Number <br />Chevron 9-57751990621 R-3 <br />Received <br />6123199 <br />San Jose, CA 95112 <br />Project Mana er <br />Christine Lillie <br />Reported <br />7/12/99 <br />- Violat7lle OxganieDx genate&C-6mpounds by EPAMeth6d'826 kQua*,Confr- <br />_ ; =Sequoia Analytical ' San�Carlos <br />Date Spike Sample QC Reporting Limit Recov RPD RPD <br />Analyte Analyzed Level Result Result Units Recov Limits % Limit % Notes* <br />Batch 9060143 <br />Date Prepared <br />6125199 <br />Extraction Method EPA 5030E JPM <br />Blank <br />9060143-BLK1 <br />1,2-Dibrotnoethane <br />6125199 <br />ND <br />ug/l <br />200 <br />1,2-Dichloroethane <br />NDty200 <br />Ethanol <br />ND <br />1000 <br />Tert-butyl alcohol <br />ND <br />200 <br />Methyl tert-butyl ether <br />,r <br />ND <br />200 <br />Di -isopropyl ether <br />ND <br />200 <br />Ethyl tett-butyl ether <br />" <br />ND <br />200 <br />Tert-amyl methyl ether <br />ND <br />200 <br />Surrogate 1,2 Dtchloroethane-d4 <br />500 <br />548 <br />760-114 <br />110 <br />Blank <br />9060143-BLK2 <br />Ethanol <br />6128199 <br />ND <br />ugll <br />1000 <br />butyl alcohol <br />" <br />ND <br />„ <br />200 <br />yl tert-butyl ether <br />ND <br />" <br />200 <br />Di -isopropyl ether <br />ND <br />200 <br />Ethyl tert-butyl ether <br />ND <br />200 <br />Tert-amyl methyl ether <br />ND <br />" <br />200 <br />Surrogate 1,2-Dtchloroethane-d4 <br />500 <br />556 <br />760-114 <br />111 <br />Blank <br />9060143-BLK3 <br />Ethanol <br />6128199 <br />ND <br />ug/l <br />1000 <br />Tert-butyl alcohol <br />ND <br />200 <br />Methyl tert-butyl ether <br />ND <br />200 <br />Di -isopropyl ether <br />ND <br />200 <br />Ethyl tert-butyl ether <br />ND <br />200 <br />Tert-amyl methyl ether <br />ND <br />200 <br />Surrogate 1 2-Dtchloroethane-d4 <br />500 <br />559 <br />760-114 <br />112 <br />LCS <br />9060143 -BSI <br />Methyl tert-butyl ether <br />6125199 <br />500 <br />447 <br />ug/l <br />700-130 <br />894 <br />Surrogate 1,2-Dtchloroethane-d4 <br />R <br />500 <br />511 <br />" <br />760-114 <br />102 <br />LCS <br />9060143-BS2 <br />Methyl tert-butyl ether <br />6128199 <br />600 <br />537 <br />ug/l <br />700-130 <br />895 _ <br />Surrogate 1,2-Dtchloroethane-d4 <br />ff500 <br />564 <br />FF <br />760-114 <br />113 <br />LCS <br />9060143-BS3 <br />Methyl test -butyl ether <br />6128/99 <br />500 <br />466 <br />ug/l <br />700-130 <br />932 <br />Surrogate 42-Dtchloroethane-d4 <br />" <br />500 <br />534 <br />760-114 <br />107 <br />Analytical - San Carlos <br />to end of report for text of notes and definitions <br />Page 9 of 11 <br />