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4 j Sequoia <br />lco Analytical <br />Imine Tech/Chevron <br />1680 Rogers Ave <br />San Jose CA 95112 <br />1455 McDowell Blvd North Ste D <br />Petaluma CA 94954 <br />(707) 792 1865 <br />FAX (707) 792-0342 <br />www sequoialabs com <br />Project Chevron Sampled 3/l/00 <br />Project Number 301 W Kettleman Lane, Lodi Received 312/00 <br />?rolect Manager Scott Boor Renorted 3123/00 <br />Volatile Organic Compounds by EPA Method 8260B/Quality Control <br />Sequoia Analytical - Petaluma <br />Date Spike Sample QC Reporting Limit Recov RPD RPD <br />Analyte Analyzed Level Result Result Units Recov Limtts % Lirrut % Notes* <br />LCS continued <br />0030090 -BSI <br />Surrogate Dtbromofluoromethane <br />314100 <br />5 00 <br />446 <br />u9/1 <br />860-118 <br />892 <br />Surrogate 12-Dtchloroethane-d4 <br />5 00 <br />457 <br />800-120 <br />914 <br />Surrogate Toluene -d8 <br />500 <br />509 <br />880-110 <br />102 <br />LCS <br />0030090-BS2 <br />Methyl tert-butyl ether <br />316100 <br />5 00 <br />498 <br />ug/l <br />727-119 <br />996 <br />Surrogate Dibromofluoromethane <br />5 00 <br />458 <br />860-118 <br />916 <br />Surrogate 1,2-Dtchloroethane-d4 <br />500 <br />480 <br />" <br />800-120 <br />960 <br />Surrogate Toluene -d8 <br />5 00 <br />493 <br />880-110 <br />986 <br />LCS <br />0030090-BS3 <br />Methyl tert-butyl ether <br />3/7/00 <br />500 <br />501 <br />ug/1 <br />727-119 <br />100 <br />Surrogate Dtbromofluoromethane <br />500 <br />4 68 <br />11860-118 <br />936 <br />Surrogate 1,2-Dtchloroethane-d4 <br />5 00 <br />551 <br />800-120 <br />110 <br />rrogaic Toluene -d8 <br />500 <br />507 <br />880-110 <br />101 <br />atria Spike <br />0030090 -MSI <br />P003009-01 <br />Methyl tort -butyl ether <br />314100 <br />25 0 <br />5 96 <br />31 9 <br />ugll <br />727-119 <br />104 <br />Surrogate Dtbromofluoromethane <br />500 <br />4 73 <br />rr860-118 <br />946 <br />Surrogate 12-Dtchloroethane-d4 <br />500 <br />492 <br />800-720 <br />984 <br />Surrogate Toluene -d8 <br />500 <br />489 <br />880-110 <br />978 <br />Matrix Spike Pup <br />0030090-MSDI <br />P003009-01 <br />Methyl tert-bury] ether <br />3/4/00 <br />25 0 <br />5 96 <br />30 8 <br />ugll <br />727-119 <br />994 20 0 4 52 <br />Surrogate Dtbromofluoromethane <br />500 <br />464 <br />860-118 <br />928 <br />Surrogate 12-Dtchloroethane-d4 <br />5 00 <br />492 <br />800-120 <br />984 <br />Surrogate Toluene -d8 <br />500 <br />510 <br />880-110 <br />102 <br />uoia Analytical - Petaluma '"Refer to end of report for text of notes and definitions <br />Page 6 of 7 <br />