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'II Client Name: ENGEO Date: 10/28/1996 Client Acct: 44200 ELAP Cert: 1386 NET Job No: 96.03008 Page: 18 Ref: 802 N. Cluff-Lodi/Project No. 4203-F1 ;I I MATRIX SPIKE / MATRIX SPIKE DUPLICATE Matrix Matrix Matrix Spike Matrix Spike Spike Dup Spike Sample Spike Dup. Date Run Sample .Parameter % Rec. % Rec. RPD Amount Conc. Cone. Conc. Flags Units Analyzed Batch Spiked METHOD 6010 (SOLID) -- " 792 269590 Antimony (ICP) -- -- -- 819.7 ND -- 'I -- NI3 mg/kg 10/23/1996 860 269590 Barium (ICP) -- -- -- 81.97 180 -- -- *M mg/kg 10/23/1996 863 269590 Beryllium (ICP) 95.9 97.1 1.2 81.97 ND 78.62 69.84 mg/kg 10/23/1996 863 269590 Cadmium (ICP) 97.4 98.8 1.4 81.97 ND 79.84, 71.09 mg/kg 10/23/1996 714 269590 1: Chromium (ICP) 106.1 113.7 6.9 81.97 20 107:+j+0 101.8 mg/kg 10/23/1996 725 269590 Chromium+6 (Color) 1.0 ND - j1 NAR mg/kg 10/18/1996 26 268894 Cobalt- (ICP) 103.6 100.3 3.2 81.97 8.3 93.22 80.42 mg/kg 10/23/1996 862 269590 Copper (ICP) 102.1 103.7 1.6 81.97 20 1035,7 94.61 mg/kg 10/23/1996 607 269590 Lead (ICP) 97.9 86.8 12.0 81.97 7.7 87.97 78.88 mg/kg 10/23/1996 607 269590 Mercury (CVAA) 104.1 106.2 2.0 0.417 0.02 0.454 0.448 mg/kg 10/28/1996 379 269769 ij Molybdenum (ICP) 96.2 95.1 1.2 81.97 ND 78.86 68.45 mg/kg 10/23/1996 661 269590 fi Nickel (ICP) 104.1 105.2 1.1 81.97 17 1021!3 92.68 mg/kg 10/23/1996 618 269590 Silver (ICP) 94.4 104.2 9.8 81.97 ND 77.42 74.97 mg/kg 10/23/1996 862 269590 Thallium (ICP) 99.9 100.3 0.3 819.7 ND 819 11 721.6 mg/kg 10/23/1996 490 269590 Vanadium (ICP) 115.0 106.1 8.1 81.97 48 142.3 124.3 mg/kg 10/23/1996 535 269590 i Zinc (ICP) 95.0 107.6 12.3 81.97 58 1359 135.4 mg/kg 10/23/1996 663 269590 TPH (Gas/BTXE,Solid) 269591 as Gasoline 107.9 107.7 0.2 2.50 ND 2.69,7 2.692 mg/kg. 10/21/1996 2071 269591 Benzene 110.6 110.5 0.1 42.85 ND 47.40 47.35 ug/kg 10/21/1996 2071 269591 M Toluene 96.7 97.2 0.5 191.10 ND 184'85 185.80 ug/kg 10/21/1996 2071 269591 LBromofluorobenzene (BURR), 113.0 114.0 0.9 100 105 113!; 114 % Rec. 10/21/1996 2071 269591 M8015 (EXT., Solid) 269591 as Diesel 93.3 88.1 5.7 16.7 1.0 16.58 15:72 mg/kg 10/23/1996 1226 269591 Ortho-terphenyl (SURR) 93.0 118.0 23.6 100 103 93 is 118 % Rec. 10/23/1996 1226 269591 8260(GCMS,Solid) 269590 Benzene 90.0 89.6 0.4 250 ND 225i1 224 ug/kg 10/23/1996 220 269590 p Chlorobenzene 92.4 91.6 0.9 250 ND 23111 229 ug/kg 10/23/1996 220 . 269590 1 1,1-Dichloroethene 84.4 87.6 3.7 250 ND 211 ii 219 ug/kg 10/23/1996 220 269590 L Trichloroethene 86.0 88.8 3.2 250 ND 215 1 222 ug/kg 10/23/1996 220 269590 Toluene 98.0 96.0 2.1 250 ND 245 240 ug/kg 10/23/1996 220 269590 4-Bromofluorobenzene (SURR) 115.0 105.0 9.1 100 98 115 j 105 % Rec. 10/23/1996 220 269590 Toluene-d8 (SURA) 111.0 99.0 11.3 100 100 111 99 % Rec. 10/23/1996 220 269590 1,2-Dichloroethane-d4 (SURR) 105.0 98.0 6.8 100 102 105 98 % Rec. 10/23/1996 220 269590 it i it !i 1i NOTE: Results apply only to the samples analyzed. Reproduction of. ths report is permitted only in its entirety.