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American Environmental Network <br />PAGE 29 <br />ENGEO INCORPORATED <br />SAMPLE ID: DP -14 <br />DATE SAMPLED: <br />05/28/97 <br />AEN LAB NO: 9705366-10 <br />DATE RECEIVED: <br />05/30/97 <br />BTEX & Gasoline HCs <br />Benzene <br />AEN WORK ORDER: 9705366 <br />REPORT DATE: <br />06/16/97 <br />ug/kg <br />CLIENT PROD. ID: 4203-F2 <br />Toluene <br />108-88-3 <br />ND <br />5 <br />ug/kg <br />06/09/97 <br />Ethylbenzene <br />100-41-4 <br />ND <br />METHOD/ REPORTING <br />DATE <br />06/09/97 <br />ANALYTE <br />CAS# RESULT LIMIT UNITS <br />ANALYZED <br />BTEX & Gasoline HCs <br />Benzene <br />EPA 8020 <br />71-43-2 <br />ND <br />5 <br />ug/kg <br />06/09/97 <br />Toluene <br />108-88-3 <br />ND <br />5 <br />ug/kg <br />06/09/97 <br />Ethylbenzene <br />100-41-4 <br />ND <br />5 <br />ug/kg <br />06/09/97 <br />" <br />Xylenes. Total <br />1330-20-7 <br />ND <br />5 <br />ug/kg <br />06/09/97 <br />Purgeable HCs as Gasoline <br />5030/GCFID <br />ND <br />1 <br />mg/kg <br />06/09/97 <br />#Extraction for TPH <br />EPA 3550 <br />- <br />Extrn Date <br />06/05/97 <br />TPH as Diesel <br />GC -FID <br />ND <br />1 <br />mg/kg <br />06/07/97 <br />TPH as Oil <br />GC -FID <br />ND <br />5 <br />mg/kg <br />06/07/97 <br />#Digestion, Metals by GFAA <br />EPA 3050 <br />- <br />Prep Date <br />05/30/97 <br />#Digestion for ICP/AA <br />EPA 3050 <br />- <br />Prep Date <br />05/30/97 <br />Volatile Organics <br />Benzene <br />EPA 8260A <br />71-43-2 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />Bromobenzene <br />108-86-1 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />Bromochloromethane <br />74-97-5 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />' <br />Bromodichloromethane <br />75-27-4 <br />ND <br />10 <br />ug/kg <br />06/04/97 <br />Bromoform <br />75-25-2 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />Bromomethane <br />74-83-9 <br />ND <br />10 <br />ug/kg <br />06/04/97 <br />n-Butylbenzene <br />104-51-8 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />sec-Butylbenzene <br />135-98-8 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />tert-Butylbenzene <br />98-06-6 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />Carbon Tetrachloride <br />56-23-5 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />Chlorobenzene <br />108-90-7 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />Chloroethane <br />75-00-3 <br />ND <br />10 <br />ug/kg <br />06/04/97 <br />Chloroform <br />67-66-3 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />Chloromethane <br />74-87-3 <br />ND <br />10 <br />ug/kg <br />06/04/97 <br />2-Chlorotoluene <br />95-49-8 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />4-Chlorotoluene <br />106-43-4 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />Dibromochloromethane <br />124-48-1 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />1,2-Dibromo-3-chloropropane <br />96-12-8 <br />ND <br />20 <br />ug/kg <br />06/04/97 <br />1,2-Dibromoethane <br />106-93-4 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />Dibromomethane <br />74-95-3 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />1,2 -Dichlorobenzene <br />95-50-1 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />1,3 -Dichlorobenzene <br />541-73-1 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />1.4 -Dichlorobenzene <br />106-46-7 <br />ND <br />5 <br />ug/kg <br />06/04/97 <br />Dichlorodifluoromethane <br />75-71-8 <br />ND <br />10 <br />ug/kg <br />06/04/97 <br />