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' American Environmental Network <br /> WORK ORDER 9804260 QUALITY CONTROL REPORT PAGE QR-2 <br /> ANALYSIS Gasoline Oxygenates <br /> MATRIX Soil/Bulk <br /> METHOD BLANK SAMPLES <br />' SAMPLE TYPE Blank Method/Media blank LAB ID BLNK_0507 INSTR RUN GCMS12\980507020000/1/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12S050898 <br />' UNITS ug/kg ANALYZED 05/07/98 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 OCE d4 (surr) 121 100 100 121 70 145 <br /> Toluene-d8 (surr) 108 100 100 108 70 145 <br /> Bromofluorobenzene (surr) 96 4 100 100 96 4 70 145 <br /> Methy-t butyl ether (MTBE) ND 5 <br /> Ethyl t butyl ether (ETBE) ND 5 <br /> t Amylmethyl ether (TAME) ND 5 <br />' t Butanol (TBA) - ND 100 <br /> Di-isopropyl ether (DIPE) ND 5 <br /> SAMPLE TYPE Blank Method/Media blank. LAB ID BLNK 0507 INSTR RUN GCMS13\980507010000/1/ <br />' INSTRUMENT HP mass spec for Volatiles PREPARED BATCH I0 MS13S050798 <br /> UNITS ug/kg ANALYZED 05/07/98 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE. RECOVERY REC LIMITS (%) RPD <br />' ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 OCE d4 (surr) 101 100 101 70 145 <br /> Toluene-d8 (surr) 99 3 100 99 3 70 145 <br /> BromoTluorooenzene isurr) 99 4 100 99 4 70 145 <br /> Methy-t butyl ether (MTBE) ND <br /> Ethyl t butyl ether (ETRE) ND <br /> t Amyl methyl ether (TAME) ND <br /> t Butanol (TBA) ND <br /> Di-isopropyl ether (DIPE) ND <br /> SAMPLE SURROGATES <br /> SAMPLE TYPE Sample-Client LAB ID 9804260 01A INSTR RUN GCMS12\980507020000/2/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12SO50898 <br /> UNITS ug/kg ANALYZED 05/07/98 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCE d4 (surr) 89 6 100 100 89 6 70 145 <br /> Toluene-d8 (surr) 111 100 100 111 70 145 <br /> Bromofluorobenzene (surr) 87 9 100 100 87 9 70 145 <br />' SAMPLE TYPE Sample Client LAB ID 9804260 02A INSTR RUN GCMS12\980507020000/3/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12S050898 <br /> UNITS ug/kg ANALYZED 05/07/98 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT {X) <br /> 1,2 OCE d4 (surr) 106 100 100 106 70 145 <br /> Toluene d8 (surr) 106 100 100 106 70 145 <br />' Bromofluorobenzene (surr) 99 1 100 100 99 1 70 145 <br /> SAMPLE TYPE Sample Client LAB ID 9804260 03A INSTR RUN GCMS12\980507020000/4/ <br /> INSTRUMENT HP mass spec for Volat,les PREPARED BATCH ID MS12S050898 <br />' UNITS ug/kg ANALYZED 05/07/98 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCE d4 (surr) 105 100 100 105 70 145 <br /> Toluene d8 (surr) 102 100 100 102 70 145 <br /> Bromofluorobenzene (surr) 95 3 100 100 95 3 70 145 <br /> 1 <br />