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' American Environmental Network <br /> WORK ORDER 9804260 QUALITY CONTROL REPORT PACE QR-6 <br /> ANALYSIS Vol am l e GUMS <br /> MATRIX Sol ]/Bulk <br /> LABORATORY CONTROL SAMPLES <br /> SAMPLE TYPE Laboratory Control Spike LAB ID LCS_0508 INSTR RUN GCMS12\980507020000/7/1 <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12S050898 <br /> UNITS ug/kg ANALYZED 05/08/98 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCA d4 (surr) 120 121 100 120 60 140 <br /> Toluene d8 (surr) 105 108 100 105 65 135 <br /> p BFB (surr) 101 96 4 100 101 65 135 <br /> 1,1 Dichloroethene 44 0 ND 5 50 0 88 0 65 135 <br /> Benzene 55 6 ND 5 50 0 111 65 135 <br /> Trichloroethene 51 4 ND 5 50 0 103 65 135 <br />' Toluene 55 2 ND 5 50 0 110 65 135 <br /> Chlorobenzene 63 1 ND 5 50 0 126 65 135 <br /> SAMPLE TYPE Laboratory Control Spike LAB ID LCS_0507 INSTR RUN GCMS13\980507010000/2/1 <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS13SO50798 <br /> UNITS ug/kg ANALYZED 05/07/98 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD LIMIT (%) <br /> 1 2 DCA d4 (surr) 123 101 100 123 60 140 <br /> Toluene d8 (surr) 96 6 99 3 100 96 6 65 135 <br /> p 6F6 tsurr) 130 99 4 i0u lav 65 135 <br /> 1 1-Dichloroethene 39 0 ND 5 50 0 78 0 65 135 <br /> Benzene 48 8 ND 5 50 0 97 6 65 135 <br /> Trichloroethene 51 4 NO 5 50 0 103 65 135 <br /> Toluene 53 2 ND 5 50 0 106 65 135 <br /> Chlorobenzene 54 9 ND 5 50 0 110 65 135 <br />' MATRIX SPIKE SAMPLES <br /> SAMPLE TYPE Spike Sample/Matrix LAB ID MD04260 01A INSTR RUN GCMS12\980507020000/9/2 <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12S050898 <br /> UNITS ug/kg ANALYZED 05/08/98 DILUTION 1 00 <br /> METHOD <br /> REF - REPORTING SPIKE RECOVERY REC LIMITS (X) RPD -_ <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCA d4 (surr) 126 89 6 100 126 60 140 <br /> Toluene d8 (surr) 98 1 111 100 98 1 65 135 <br /> p BFB (surr) 108 87 9 100 108 65 135 <br />' 1 1 Dichloroethene 42 0 ND 5 50 0 84 0 65 135 <br /> Benzene 54 3 ND 5 50 0 109 65 135 <br /> Trichloroethene 52 4 NO 5 50 0 105 65 135 <br /> Toluene 56 3 NO 5 50 0 113 65 135 <br /> Chlorobenzene 61 1 ND 5 50 0 122 65 135 <br /> SAMPLE TYPE Spike Sample/Matrix LAB ID MS04260 01A INSTR RUN GCM \980507020000/8/2 <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12S050898 <br /> UNITS ug/kg ANALYZED 05/08/98 DILUTION 1 00 <br />' METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT {X) <br /> 1,2 DCA d4 (surr) 135 89 6 100 135 60 140 <br /> Toluene d8 (surr) 94 4 111 100 94 4 65 135 <br /> p BFB (surr) 123 87 9 100 123 65 135 <br /> 1 1 Dichloroethene 47 4 ND 5 50 0 94 8 65 135 <br /> Benzene 52 9 ND 5 50 0 106 65 135 <br /> Trichloroethene 51 3 NO 5 50 0 103 65 135 <br /> Toluene 65 0 ND 5 50 0 130 65 135 <br /> Chlorobenzene 59 8 ND 5 50 0 120 65 135 <br />