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GeoAnalytical Laboratories, Inc. <br />1405 Kansas Avenue Modesto, CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br />D 9/19/03 <br />port # P25$-13 <br />Amnt Spiked <br />CERTIFICATE DF ANALYSIS <br />ate. <br />100 <br />othill Engineering <br />2-Bromo-l-chloropropane <br />100 <br />Date Recd: <br />Date Started: <br />9/15/03 <br />9/18/03 <br />12793 Paddy Creek Lane <br />Project: 3rd Quarter 2003 <br />Dat 'Completed:9/18/03 <br />. !rf. <br />Lodi CA <br />95240 <br />Donna Keller <br />Certification # 1157 <br />Laboratory Director <br />Date Sampled: <br />9/11/03 <br />PQ## <br />Time. <br />12:48 pm <br />Sample ID: GMX-1 <br />Sampler: <br />Lab ID: P308529 <br />Method <br />RL <br />Analyte <br />Results <br />Units <br />82606 <br />6 <br />Benzene <br />65 <br />µg/L <br />6 <br />Toluene <br />430 <br />6 <br />Ethyl Benzene <br />1810 <br />12 <br />Total Xylenes <br />5160 <br />10 <br />Methyl tert-butyl ether (MTBE) <br />ND <br />800 <br />Ethanol <br />ND <br />100 <br />tert-Butanol <br />ND <br />10 <br />di -Isopropyl ether (DIPE) <br />ND <br />10 <br />Ethyl tert-butyl ether (ETBE) <br />ND <br />10 <br />tert-Amyl methyl ether (TAME) <br />., <br />ND <br />• <br />Mario D'Onofrio <br />Chemist <br />Surrogate <br />Amnt Spiked <br />Amnt Rec. % Recovery OC Limit % <br />1,2-Dichloroethane-d4 <br />100 <br />119 119.0 72-132 <br />2-Bromo-l-chloropropane <br />100 <br />78.2 78.2 71-134 <br />4-Bromofluorobenzene <br />100 <br />105 105.0 74-132 <br />Donna Keller <br />Certification # 1157 <br />Laboratory Director <br />