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is <br />Surrogate <br />GeoAnalytical Laboratories, <br />Inc. <br />1405 Kansas Avenue Modesto, CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br />5.00 <br />eport # P258-13 <br />CERTIFICATE OF ANALYSIS <br />Date: <br />9/19/03 <br />0 oothill Engineering <br />4-Bromofluorobenzene <br />5.00 <br />Date Rec'd: <br />Date Started: <br />9/15/03 <br />9/18/03 <br />12793 Paddy Creek Lane <br />Project: 3rd Quarter 2003 <br />Date Completed:9/ 18/03 <br />Lodi CA <br />95240 <br />Date Sampled: <br />9/11/03 <br />PQ# <br />Time: <br />10:40am <br />Sample ID: MW -3 <br />Chemist <br />Certification # 1157 <br />Sampler <br />Laboratory Director <br />Lab 1D: P308531 <br />Method <br />RL <br />Analyte <br />Results <br />Units <br />8260B <br />0.3 <br />Benzene <br />ND <br />ug/L <br />0.3 <br />Toluene <br />ND <br />0.3 <br />Ethyl Benzene <br />ND <br />0.6 <br />Total Xylenes <br />ND <br />0.5 <br />Methyl tert-butyl ether (MTBE) <br />ND <br />40 <br />Ethanol <br />ND <br />5 <br />tert-Butanol <br />ND <br />0.5 <br />di -isopropyl ether (D1PE) <br />ND <br />0.5 <br />Ethyl tert-butyl ether (ETBE) <br />ND <br />0.5 <br />tert-Amyl methyl ether (TAME) <br />ND <br />is <br />Surrogate <br />Amnt Spiked <br />Amnt Rec• % Recovery QC Limit % <br />1,2-Dichloroethane-d4 <br />5.00 <br />5.29 105.8 72-132 <br />2-Bromo-l-chloropropane <br />5.00 <br />4.28 85.6 71-134 <br />. <br />4-Bromofluorobenzene <br />5.00 <br />4.59 91.8 74-132 <br />lario <br />D' not <br />Donna Keller <br />Chemist <br />Certification # 1157 <br />Laboratory Director <br />