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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209)572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# N058-03 Oxygenates Date: 3/05/02 <br /> Foothill Engineering Project: Sunwest Liquors Date Ree'd: 2/27/02 <br /> Date Started: 2/28/02 <br /> 12793 Paddy Creek Lane <br /> Lodi CA 95240 PO# Date Completed:3/01/02 <br /> Date Sampled: 2/26/02 <br /> Sampler: Andria Light <br /> Sample ID Lab ID RL Method Analyte Results Units <br /> MW-4 N302215 1.0 8260B Methyl tert-butyl ether(MTBE) ND pg/L <br /> 40 Ethanol ND <br /> 20 Cert-Butanol ND <br /> 1.0 di-Isopropyl ether(DIPE) ND <br /> 1.0 Ethyl tert-butyl ether(ETBE) ND <br /> 1.0 tert-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 5.00 4,02 80.4 72-132 <br /> 2-Bromo-l-chloropropane 5.00 4.21 84.2 71-134 <br /> 4-Bromofluorobenzene 5.00 4.63 92.6 74-132 <br /> 4tW-3 N302216 1.0 8260B Methyl tert-butyl ether (MTBE) 1.6 lig/L <br /> 40 Ethanol ND <br /> 20 tert-Butanol ND <br /> 1.0 di-Isopropyl ether(DIPE) ND <br /> 1.0 Ethyl tert-butyl ether (ETBE) ND <br /> 1.0 tert-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d9 5,00 4.15 83 72-132 <br /> 2-Bromo-1-chloropropane 5.00 4.32 86.4 71-134 <br /> 4-Bromofluorobenzene 5.00 4.44 88.8 74-132 <br /> MW-2 N302217 20 8260B Methyl tert-butyl ether (MTBE) ND lig/L <br /> 800 Ethanol ND <br /> 400 tert-Butanol ND <br /> 20 di-Isopropyl ether(DIPE) ND <br /> 20 Ethyl tert-butyl ether (ETBE) ND <br /> 20 tert-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 100 87.3 87.3 72-132 <br /> 2-Bromo-l-chloropropane 100 108 108 71-134 <br /> 4-Bromofluorobenzene 100 102 102 74-132 <br /> Elevated detection limits due to high level of non-target analytes. <br /> Mario D'Onofrio Donna Keller <br />