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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto, CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# M178-06 Oxygenates Date: 7/03/01 <br /> Date Rec'd: 6/27/01 <br /> Foothill Engineering Project: 2nd,QTR,2001 G.W. Date Started: 7/02/01 <br /> 12793 Paddy Creek Lane Date Completed: 7/03/01 <br /> Lodi CA 95240 PO# <br /> Date Sampled: 6/26/01 <br /> Time: <br /> Sampler: Don Light <br /> Sample ID: Trip Blank <br /> Lab ID: M306358 <br /> Method RL Analyte Results Units <br /> 8260B 1.0 Methyl tert-butyl ether (MTBE) ND pg/L <br /> 10 Ethanol ND <br /> 10 tert-Butanol ND <br /> 1.0 di-Isopropyl ether (DIPS) ND <br /> 1.0 Ethyl tent-butyl ether (ETBE) ND <br /> 1.0 tert-Amyl methyl ether (TAME) ND <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% <br /> 1,2-Dichloroethane-d, 5.00 4.98 99.6 72-132 <br /> • 2-Bromo-1-chloropropane 5.00 4.33 86.6 71-134 <br /> 4-Bromofluorobenzene 5.00 5.56 111.2 74-132 <br /> Mario D'Onofricv Donna Keller <br /> Chemist Certification # 1157 Lahoratory Director <br />