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�NN Submission 2004-06-0835 <br /> Fuel Oxygenates by 8260B <br /> ' Philip Services- Illinois <br /> Attn Mark Miiward <br /> 210 W Sand Bank Road <br /> Colombia. IL 62236 <br /> ' Phone (618)281-1547 Fax (618) 281-5120 <br /> Project Earthgrains Received 06/25/2004 17 07 <br /> ' � 'Q <br /> �w —�fz we.,,, a"�L.,q,�r � i S Y <br /> Batc"tt Qt'i'Re Olt �tR� 1� � - ` <br /> Prep(s) <br /> 50306 <br /> a <br /> -8260E3 <br /> iK'Z 'w«�'w 4 <br /> Laboratory ControlrSpike -SoilC <br /> a s <br /> �Q Batch#,2004107/06=02 62 <br /> � a. �� <br /> LCS 2004/07/06702 62-019',,,- '� ' E� Eztrac'ted 0710612004_<�, natyzed 0710612004=17 19 <br /> LCSD 2D04/07/06,02'62_045,--,'-,,,t - <Extracted"07/[}6/2004 A A'rialyzed 507/06/2004,17 45 <br /> Compound Conc ug/Kg Exp Conc Recovery% RPD Ctrl Limits% Flags <br /> LCS LCSD LCS LCSD % Rec I RPD LCS LCSD <br /> Methyl Cert-butyl ether(MTBE) 443 460 500 886 920 38 65-165 20 <br /> Benzene 51 8 52 0 500 1036 1040 04 69-129 20 <br /> Toluene 516 531 500 1032 1062 2 9 70-130 20 <br /> Surrogates(s) <br /> 1,2-Dichloroethane-d4 421 411 500 84 2 822 72-124 <br /> Toluene-d8 510 506 500 11020 11012 75-116 <br /> 1 <br /> 1 <br /> Severn Trent Laboratories, Inc 07/08/2004 08 53 <br />' STL San Francisco`1220 Quarry Lane Pleasanton CA 94566 <br /> A part of Severe Trent Plc Tel 925 484 1919 Fax 925 484 1096"www sti-inc corn"CA OHS ELAP#2496 Page 23 of 26 <br />