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Analytical Data <br /> • <br /> Client Philips Environmental Services Corp Job Number 720-450-1 <br /> Client Sample ID SP-1 <br /> Lab Sample ID 720-450-8 Date Sampled 11/10/2005 1506 <br /> Client Matrix Water Date Received 11/11/2005 2015 <br /> 8260B Volatile Organic Compounds by GCIMS <br /> Method 82606 Analysis Batch 720-2007 Instrument ID Varian 3900C <br /> Preparation 5030E Lab File ID c Isaturnwsldata1200511111 <br /> Dilution 10 Initial WeightNolume 10 mL <br /> Date Analyzed 11/16/2005 1433 Final WeightNolume 10 mL <br /> Date Prepared 11/16/2005 1433 <br /> Analyte Result(ug1L) Qualifier RL <br /> 1,2-Dichloroethane ND 50 <br /> Benzene 880 5 0 <br /> Ethylbenzene 500 5 0 <br /> MTBE ND 5 0 <br /> TAME 15 5 0 <br /> Toluene 200 5 0 <br />' Xylenes,Total 2100 10 <br /> TBA ND 50 <br /> DIPE 21 10 <br /> Gasoline Range Organics(GRO)-05-C12 16000 500 <br /> Ethyl tert-butyl ether ND 5 0 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8 107 77- 121 <br /> 1,2-Dichloroethane-d4 113 73- 130 <br /> STL San Francisco Page 11 of 34 <br />