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Quality Control Results <br /> Client Philips Environmental Services Corp Job Number 720-450-1 <br /> Matrix Spike/ Method 8260B <br /> Matrix Spike Duplicate Recovery Report-Batch 720-2007 Preparation 5030B <br /> S� { li 0�IS *YN1'4A1 de}, lI� <br /> �L <br /> MS Lab Sample ID 720-450-8 G Analysis Batch 720-2007 Instrument ID Varian 3900C <br /> Client Matrix Water Prep Batch NIA Lab File ID c Isaturnwsldata12005111 <br /> Dilution 10 Initial WeightNolume 10 mL <br /> Date Analyzed 11/16/2005 1501 Final Weight/Volume 10 mL <br /> Date Prepared 11/16/2005 1501 <br /> MSD Lab Sample ID 720-450-8 Analysis Batch 720-2007 Instrument ID Varian 3900C <br /> Client Matrix Water Prep Batch NIA Lab File ID c Isatumwsldata1200511\1 <br /> Dilution 10 Initial Weight/Volume 10 mL. <br /> Date Analyzed 11/16/2005 1528 Final Weight/Volume 10 mL <br /> Date Prepared 11/16/2005 1528 <br /> % Rec <br /> Analyte ��� Ms MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Benzene <br /> I 51 39 69-129 3 20 N N <br /> 1 <br /> MTBE U ��' 94 87 65-165 7 20 <br /> Toluene a 89 76 70-130 8 20 <br /> Surrogate MS% Rec MSD%Ree Acceptance Limits <br /> 1 Toluene-d8 110 106 77-121 <br /> 1,2-Dichloroethane-d4 113 107 73-130 <br /> 1 <br /> 1 <br /> • <br /> Calculations are performed before rounding to avoid round-off errors in calculated results <br /> STL San Francisco Page 23 of 34 <br />