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J <br /> Quality Control Results <br /> Client Philips Environmental Services Corp Job Number 720450-1 <br /> Matrix Spike/ Method 8260B <br /> Matrix Spike Duplicate Recovery Report-Batch 720-2234 Preparation 50308 <br /> MS Lab Sample ID 720-450-95$ ` Analysis Batch 720-2234 � I��I` Instrument ID Saturn 2100 <br /> Client Matrix Water Prep Batch NIA " � Lab File ID d ldata1200511\11210517. <br /> Dilution 10 Initial WeightNolume 10 mL <br /> Date Analyzed 11/21/2005 0853 Final WeightNolume 10 mL <br /> Date Prepared 11/21/2005 0853 <br /> MSD Lab Sample ID 720-450-9 Analysis Batch 720-2234 Instrument ID Saturn 2100 <br /> Client Matrix Water Prep Batch NIA Lab File ID d ldata1200511\112105172[ <br /> Dilution 10 Initial WeightNolume 10 mL <br /> Date Analyzed 11/21/2005 0919 Final WeightNolume 10 mL <br /> Date Prepared 11/21/2005 0919 <br /> 1 %Rec <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1 Benzene 112 113 69-129 1 20 <br /> MTBE 90 90 65-165 1 20 <br /> Toluene 106 105 70-130 1 20 <br /> Surrogate MS% Rec MSD%Rec Acceptance Limits <br /> Toluene-d8 103 104 77- 121 <br /> 1,2-Dichloroethane-d4 80 79 73-130 <br /> 1 <br /> • <br /> Calculations are performed before rounding to avoid round-off errors in calculated results <br /> STL San Francisco Page 31 of 34 <br />