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® STL Submission# 2003-02-0137 <br /> Fuel Oxygenates by 82608 <br /> Philip Services- Illinois <br /> Attn Mark Mllward <br /> 210 W Sand Bank Road <br /> Colombia, IL 62236 <br /> Phone (618) 281-1547 Fax (618)281-5120 <br /> Project C23484517BOO Received 02/07/2003 11 40 <br /> Sara Lee <br /> Batch QC Report <br /> Prep(s) 5030E Test(s) 8266B ; <br /> w <br /> Laboratory Control Spike Water QC Batch#2003102112-01 27 <br /> LCS 2003102112-01 27-004 Extracted 02/12/2003 Analyzed 021121200311 29 <br /> ,LCSD 2003102112-01 27-005 Extracted 02/12/2003 Analyzed 021121200311 56 i <br /> Compound Conc ug/L Exp Conc Recovery RPD Ctrl Limits% Flags <br /> LCS LCSD LCS LCSD % Rec RPD LCS LCSD <br /> Methyl tert-butyl ether(MTBE) 312 301 250 1248 120 4 36 65-165 20 <br /> Benzene 25 3 25 3 25 0 1012 1012 00 69-129 20 <br /> Toluene 247 24 6 25 0 988 98 4 04 70-130 20 <br /> Surrogates(s) <br /> 1 2-Dichloroethane-d4 562 527 500 1124 1054 76-114 <br /> Toluene-d8 482 490 500 964 980 88-110 <br /> 1 Severn Trent Laboratories, Inc 02/14/2003 15 05 <br /> STL San Francisco' 1220 Quarry Lane Pleasanton CA 94566 <br /> A part Of Severn hent Pic Tel 925 484 1919 Fax 925 484 1096 a www stl-inc eom'CA DHS ELAP#2496 Page 24 of 28 <br />