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® Submission # 2003-02-0137 <br /> STL <br /> Fuel Oxygenates by 8260B <br /> Philip Services- Illinois <br /> Attn Mark Mllward <br /> 210 W Sand Bank Road <br /> Colombia, IL 62236 <br /> Phone (618) 281-1547 Fax (618)281-5120 <br /> Project C23484517B00 Received 02/07/2003 11 40 <br /> Sara Lee <br /> Batch QC Report <br /> Prep(s) 50306 - - Test(s) 8260E <br /> Matrix Spike ( MS I MSD Water QC Batch# 2003102112-01 27 <br /> MW-3 >> MS Lab ID 2003-02-0137-003 <br /> 1 MS 2003/02/12-0127-009 Extracted 02/12/2003 Analyzed 02/12/2003 13 23 <br /> Dilution 1 00 <br /> i MSD 2003102112-01 27-010 Extracted 02/12/2003 Analyzed 02/12/2003 13 48 <br /> Dilution 1 00 <br /> Compound Conc ug/L pk Leve Recovery Limits% Flags <br /> MS MSD Sample ug/L MS MSD RPD Rec RPD MS MSD <br /> Methyl tent-butyl ether 278 289 ND 250 1112 1156 39 65-165 20 <br /> Benzene 249 241 ND 250 996 964 3 3 69-129 20 <br /> Toluene 247 23 9 ND 250 988 966 33 70-130 20 <br /> Surrogate(s) <br /> 1 2-Dichloroethane-d4 522 521 500 1044 1042 76-114 <br /> Toluene-d8 503 481 500 1 10o5 1961 88-110 <br /> l <br /> 1 <br /> I <br /> 1 Severn Trent Laboratories, Inc 02114/2003 15 05 <br /> STL San Francisco'1220 Quarry Lane Pleasanton CA 94566 <br /> A part or Severn Trent Pic Tel 925 484 1919 Fax 925 484 1096'www stl-inc com a CA DNS ELAP*2496 Page 27 of 28 <br />