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Submission # 2002-11-0161 <br /> Fuel Oxygenates by 8260B <br /> STL San Francisco <br /> Philip Services- Illinois 1220 Quarry Lane <br /> Attn Mark Milward Pleasanton CA 94566 <br /> 210 W Sand Bank Road Tel (925)484-1919 <br /> Colombia IL 62236 Fax (925)484-1096 <br /> Phone (618) 281-1547 Fax (618) 281-5120 www stl-inc corn <br /> Project BOOC23484517 Received 11/07/2002 12 20 www chrornalab corn <br /> Sara Lee (STKD) CA DHS FLAP#2496 <br /> Batch QC Report <br /> Prep(s) 50308 Test(s) 8260FAB <br /> Laboratory Control Spike Water QC Batch#2002111114-01 27 <br /> ILCS 2002111114-01 27-004 Extracted 11114/2002 Analyzed 11/14/2002 11 22 <br /> LCSD 2002111114-01 27-005 Extracted 11/14/2002 Analyzed 111141200211 44 <br /> Conc ug/ Exp Conc Recovery RPD Ctr! Limits% Flags <br /> Compound LCS LCSD LCS LCSD % Rec RPD LCS LCSD <br /> Benzene 21 0 20 7 250 840 828 1 4 69-129 20 <br /> >� Toluene 22 6 223 1250 90 4 892 1 3 70-130 20 <br /> Methyl tent-butyl ether(MTBE) 19 9 227 25 0 796 908 131 65-165 20 <br /> Surrogates(s) <br /> I 2-Dichloroethane-d4 476 439 500 952 878 76-114 <br /> Toluene-d8 507 505 500 1014 1010 88-110 <br /> L <br /> L <br /> 11/22/2002 14 37 <br /> STL San Francisco is part of Severn Trent Laboratories Inc Page 16 of 18 <br />