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AN ENVIRONMENTAL ANALYTICAL LABORATORY <br />Client Sample ID: FMS24DP01-01-NS Lab Duplicate <br />Lab ID#: 0710143-01AA <br />J = Estimated value due to bias in the CCV. <br />Container Type:1 Liter Summa Canister <br />Method <br />Surrogates %Recovery Limits <br />Toluene -d8 104 70-130 <br />1,2-Dich loroethane-d4 105 70-130 <br />4-Bromofluorobenzene 88 70-130 <br />Page 10 of 26 <br />Rpt- Limit <br />Amount <br />Rpt. Limit <br />Amount <br />Compound <br />(ppbv) <br />(ppbv) <br />(uG1m3) <br />(uGlm3) <br />1,1,2 -Trichloroethane <br />1.2 <br />Not Detected <br />6.4 <br />Not Detected <br />Tetrachloroethene <br />1.2 <br />8.3 <br />7.9 <br />56 <br />2-Hexanone <br />4.7 <br />Not Detected <br />19 <br />Not Detected <br />Dibromochloromethane <br />1.2 <br />Not Detected <br />9.9 <br />Not Detected <br />1,2-Dibromoethane (EDB) <br />1.2 <br />Not Detected <br />9.0 <br />Not Detected <br />Chiorobenzene <br />1.2 <br />Not Detected <br />5.4 <br />Not Detected <br />Ethyl Benzene <br />1.2 <br />1.2 <br />5.0 <br />5.4 <br />m,p-Xylene <br />1.2 <br />4.3 <br />5.0 <br />18 <br />o -Xylene <br />1.2 <br />1.5 <br />5.0 <br />6.4 <br />Styrene <br />1.2 <br />Not Detected <br />5.0 <br />Not Detected <br />Bromoform <br />1.2 <br />Not Detected <br />12 <br />Not Detected <br />Cumene <br />1.2 <br />Not Detected <br />5.7 <br />Not Detected <br />1,1,2,2 -Tetrachloroethane <br />1.2 <br />Not Detected <br />8.0 <br />Not Detected <br />Propylbenzene <br />1.2 <br />Not Detected <br />5.7 <br />Not Detected <br />4-Ethyltoluene <br />1.2 <br />1.4 <br />5.7 <br />7.0 <br />1,3,5-Tdmethylbenzene <br />1.2 <br />Not Detected <br />5.7 <br />Not Detected <br />1,2,4 Trimethylbenzene <br />1.2 <br />1.6 <br />5.7 <br />8.1 <br />1,3 -Dichlorobenzene <br />1.2 <br />Not Detected <br />7.0 <br />Not Detected <br />1,4 -Dichlorobenzene <br />1.2 <br />Not Detected <br />7.0 <br />Not Detected <br />alpha-Chlorotoluene <br />1.2 <br />Not Detected <br />6.0 <br />Not Detected <br />1,2 -Dichlorobenzene <br />1.2 <br />Not Detected <br />7.0 <br />Not Detected <br />1,2,4 Trichlorobenzene <br />4.7 <br />Not Detected <br />34 <br />Not Detected <br />Hexachlorobutadiene <br />4.7 <br />Not Detected <br />50 <br />Not Detected <br />isobutane <br />12 <br />Not Detected <br />28 <br />Not Detected <br />Propane <br />4.7 <br />5.1 <br />8.4 <br />9.2 <br />J = Estimated value due to bias in the CCV. <br />Container Type:1 Liter Summa Canister <br />Method <br />Surrogates %Recovery Limits <br />Toluene -d8 104 70-130 <br />1,2-Dich loroethane-d4 105 70-130 <br />4-Bromofluorobenzene 88 70-130 <br />Page 10 of 26 <br />