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Laboratories Inc.��i� <br />Environmental Testing Laboratory Since 1949 <br />Environmental Cost Management Reported: 08/25/2014 9:59 <br />3525 Hyland Ave Project: CA ARNG Stockton CSMS <br />Costa Mesa, CA 92626 Project Number: [none] <br />Project Manager: Don Stevens <br />Polynuclear Aromatic Hydrocarbons (EPA Method 8270C -SIM) <br />Quality Control Report - Precision & Accuracy <br />Control Limits <br />Source Source Spike Percent Percent Lab <br />Constituent Type Sample ID Result Result Added Units RPD Recovery RPD Recovery Quals <br />QC Batch ID: BXG0310 <br />Used client sample: <br />N <br />Acenaphthene <br />MS <br />1411671-62 <br />ND <br />0.027333 <br />0.033670 <br />mg/kg <br />81.2 <br />50-130 <br />MSD <br />1411671-62 <br />ND <br />0.030272 <br />0.033557 <br />mg/kg <br />10.2 <br />90.2 <br />30 <br />50-130 <br />Acenaphthylene <br />MS <br />1411671-62 <br />ND <br />0.028667 <br />0.033670 <br />mg/kg <br />85.1 <br />52-130 <br />MSD <br />1411671-62 <br />ND <br />0.031248 <br />0.033557 <br />mg/kg <br />8.6 <br />93.1 <br />30 <br />52-130 <br />Anthracene <br />MS <br />1411671-62 <br />ND <br />0.030000 <br />0.033670 <br />mg/kg <br />89.1 <br />52-130 <br />MSD <br />1411671-62 <br />ND <br />0.033527 <br />0.033557 <br />mg/kg <br />11.1 <br />99.9 <br />30 <br />52-130 <br />Benzo[a]anthracene <br />MS <br />1411671-62 <br />ND <br />0.029667 <br />0.033670 <br />mg/kg <br />88.1 <br />52-130 <br />MSD <br />1411671-62 <br />ND <br />0.032550 <br />0.033557 <br />mg/kg <br />9.3 <br />97.0 <br />30 <br />52-130 <br />Benzo[b]fluoranthene <br />MS <br />1411671-62 <br />ND <br />0.029667 <br />0.033670 <br />mg/kg <br />88.1 <br />40-130 <br />MSD <br />1411671-62 <br />ND <br />0.032876 <br />0.033557 <br />mg/kg <br />10.3 <br />98.0 <br />30 <br />40-130 <br />Benzo[k]fluoranthene <br />MS <br />1411671-62 <br />ND <br />0.031000 <br />0.033670 <br />mg/kg <br />92.1 <br />40-130 <br />MSD <br />1411671-62 <br />ND <br />0.034178 <br />0.033557 <br />mg/kg <br />9.8 <br />102 <br />30 <br />40-130 <br />Benzo[a]pyrene <br />MS <br />1411671-62 <br />ND <br />0.032000 <br />0.033670 <br />mg/kg <br />95.0 <br />40-130 <br />MSD <br />1411671-62 <br />ND <br />0.035805 <br />0.033557 <br />mg/kg <br />11.2 <br />107 <br />30 <br />40-130 <br />Benzo[g,h,i]perylene <br />MS <br />1411671-62 <br />ND <br />0.026333 <br />0.033670 <br />mg/kg <br />78.2 <br />20-130 <br />MSD <br />1411671-62 <br />ND <br />0.028644 <br />0.033557 <br />mg/kg <br />8.4 <br />85.4 <br />30 <br />20-130 <br />Chrysene <br />MS <br />1411671-62 <br />ND <br />0.029333 <br />0.033670 <br />mg/kg <br />87.1 <br />40-130 <br />MSD <br />1411671-62 <br />ND <br />0.032225 <br />0.033557 <br />mg/kg <br />9.4 <br />96.0 <br />30 <br />40-130 <br />Dibenzo[a,h]anthracene <br />MS <br />1411671-62 <br />ND <br />0.025333 <br />0.033670 <br />mg/kg <br />75.2 <br />40-130 <br />MSD <br />1411671-62 <br />ND <br />0.028644 <br />0.033557 <br />mg/kg <br />12.3 <br />85.4 <br />30 <br />40-130 <br />Fluoranthene <br />MS <br />1411671-62 <br />ND <br />0.030333 <br />0.033670 <br />mg/kg <br />90.1 <br />40-130 <br />MSD <br />1411671-62 <br />ND <br />0.033201 <br />0.033557 <br />mg/kg <br />9.0 <br />98.9 <br />30 <br />40-130 <br />Fluorene <br />MS <br />1411671-62 <br />ND <br />0.028667 <br />0.033670 <br />mg/kg <br />85.1 <br />40-130 <br />MSD <br />1411671-62 <br />ND <br />0.031574 <br />0.033557 <br />mg/kg <br />9.7 <br />94.1 <br />30 <br />40-130 <br />Indeno[1,2,3-cd]pyrene <br />MS <br />1411671-62 <br />ND <br />0.026333 <br />0.033670 <br />mg/kg <br />78.2 <br />30-130 <br />MSD <br />1411671-62 <br />ND <br />0.028970 <br />0.033557 <br />mg/kg <br />9.5 <br />86.3 <br />30 <br />30-130 <br />Naphthalene <br />MS <br />1411671-62 <br />ND <br />0.024667 <br />0.033670 <br />mg/kg <br />73.3 <br />50-130 <br />MSD <br />1411671-62 <br />ND <br />0.027017 <br />0.033557 <br />mg/kg <br />9.1 <br />80.5 <br />30 <br />50-130 <br />Phenanthrene <br />MS <br />1411671-62 <br />ND <br />0.028000 <br />0.033670 <br />mg/kg <br />83.2 <br />40-130 <br />MSD <br />1411671-62 <br />ND <br />0.030597 <br />0.033557 <br />mg/kg <br />8.9 <br />91.2 <br />30 <br />40-130 <br />Pyrene <br />MS <br />1411671-62 <br />ND <br />0.030333 <br />0.033670 <br />mg/kg <br />90.1 <br />40-130 <br />MSD <br />1411671-62 <br />ND <br />0.033527 <br />0.033557 <br />mg/kg <br />10.0 <br />99.9 <br />30 <br />40-130 <br />Nitrobenzene -d5 (Surrogate) <br />MS <br />1411671-62 <br />ND <br />0.11267 <br />0.13468 <br />mg/kg <br />83.7 <br />30-110 <br />MSD <br />1411671-62 <br />ND <br />0.12727 <br />0.13423 <br />mg/kg <br />12.2 <br />94.8 <br />30-110 <br />2-Fluorobiphenyl (Surrogate) <br />MS <br />1411671-62 <br />ND <br />0.11400 <br />0.13468 <br />mg/kg <br />84.6 <br />40-120 <br />MSD <br />1411671-62 <br />ND <br />0.13020 <br />0.13423 <br />mg/kg <br />13.3 <br />97.0 <br />40-120 <br />The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. <br />All results listed in this report are for the exclusive use of the submitting <br />party. BC Laboratories, Inc. assumes no responsibility <br />for report alteration, separation, detachment or third <br />party interpretation. <br />Report ID: 1000268115 <br />4100 Atlas <br />Court Bakersfield, <br />CA 93308 (661) 327-4911 FAX (661) <br />327-1918 <br />www.bclabs.com <br />Page 11 of 25 <br />