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GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock,CA 95380 Phone(209)669-0100 Fax(209)668-8516 <br /> email: lab.geo@att.net <br /> Date: 05/08i09 <br /> Report 1* MUM Project: . <br /> I Date Rcc'd: 05/04/09 <br /> Dale Huff <br /> 4447 South Airport Way PO#: <br /> Stockton,CA . <br /> Semi-Volatile Organic Chemistry of Hazardous Waste-Quality Control <br /> GeoAnalytical Laboratories, Inc. <br /> Reporting Spike Source %REC RPU <br /> AnAN-tc Result Limit Units Level Result %REC Limits RPD Limit Note, <br /> Batch V001166-3510B(Shake Out) Prepared:05/05/09 Analyzed:05/06/09 <br /> 4 U-S(V001166-BSI) <br /> I'.4=Crichlorohenzene 35.2 2.0 ug/L 300.0 35 46-109 <br /> 1.4-Dichlorobenzene 32.9 2.0 100.0 33 37-113 <br /> 2,4-Dinitrotoluene 64.1 2.0 100.0 64 33-135 <br /> 2-Chlorophenol 60.7 2.0 150.0 40 38-117 <br /> 4-C'hloro-3-me1hylphenol 72.6 4.0 150.0 48 44-127 <br /> 4-Nitrophenol 56.7 10.0 150.0 38 16-105 <br /> Acenaphthene 45,0 2.0 100.0 45 42-115 <br /> N-Nitrosodi-n-propyl4minc 47.2 2.0 100.0 47 37447 <br /> 11cwachloruplrenui 118 10.0 150.0 79 55-138 <br /> Phcliol 28.9 2.0 150.0 19 6-93 <br /> P.relic 57.3 2.0 100.0 57 38-140 <br /> .Sarrugole:1,4,6-Tribromophenol _- _ 89.6 - - - 150.0 '_ 60 10-123 <br /> Surrogare:2-Fluerobiphenyl 40.7 100.0 41 43-141 <br /> Surrogarr:1-Fluorophenol 41-3 150.0 18 11-100 <br /> Surrogare;Nitrobenzene-4 40.0 100.0 40 35-141 <br /> Surrak rue, Phenol-d6 30.8 150.0 11 10-94 <br /> Soar{Kure:p-7erphenyl-d14 66.6 100.0 67 33-141 <br /> LCS Du V001166-.BSD1 <br /> 1.2.4-Trichlorobenzene 55.2 2.0 ug/L 100.0 55 46-109 44 16 <br /> l.4-Dichlorobenzene 50.7 2.0 100.0 51 37413 43 15 <br /> 2.4-Dinitrotoluene 96.0 2.0 100.0 96 33-135 40 14 <br /> 2-Chlorophenol 94.6 2.0 150.0 63 38-117 44 21 <br /> 4-Chloror3-methyiphenol 119 4.0 150.0 8o 44-127 49 24 <br /> 4-Nitrophenol 73.2 10.0 150.0 49 16-105 25 13 <br /> Acenaphthene 71.4 2.0 100.0 71 42-115 45 16 <br /> N-Nitrosodi-n-propylamine 77.3 2.0 100.0 77 37-147 48 20 <br /> Pentachlorophenol 156 10.0 150.0 104 55-138 28 16 <br /> Phenol 53.0 2.0 150.0 35 6-93 59 18 <br /> 11%.rcne .64.0 2.0 100.0 64 38-140 11 18 <br /> Surrugwe ?4.6-Tribromophenol 137 150.0 92 10-113 <br /> Surrugare:2-Fhmrobiphenyl 63.4 100.0 63 43-141 <br /> Surrogate-?-Fluoropherrol 67.5 150.0 45 11-100 <br /> Surrogare:Nitrobenzene-d5 63.4 100.0 63 35-141 <br /> Surrogrue.Phenol46 54.1 150.0 36 10-94 <br /> Surrugare;p-Terpherryl-d14 65.1 100.0 65 33-141 <br /> Certification#2585 <br />