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CWirotnie Ltepartment Oi +nxi1., SuDsianees Control 'A Number: A;uoaasB o Hazardous Materials Laboratory i + to AN00470 a Inorganic Section Quality Assurance Summary for ICP N N HML Sag OC Sample Method Calibration VeriRcation Duplicate Spiked Sample HML NO.: AN0047T Matrix: SOLID ht M Blank Standard d Element mg/kg mglL Spike Resuhs mglkg Unspiked Spike %Recovery Result Added N round known % found known % A: 3: RPD Img/kg) (mglkgl A: B; m T) rng/kg M As-Arsenic 67.D 68.2 98.2 <0.10 10.2 I0.0 102 509 504 0.99 75.00 500 302 t01 m p Ba-Barium 47.2 50.6 93.3 <0.010 9.74 10-0 97.4 582 553 6.19 59.3 --- _T 00 105 98.7 z Be-BeryfGum 4.01 4.11 97.fi 70.005 2.02 2.00 101 104 104 0.00 <0.25 100 104 l0q Cd-Cadmium 19.6 19.3 102 <0.010 10.7 10.0 107 531 529 O.OD 70.50 500 706 106 d Co�abalt 22.0 2i.9 100 70.05 10.5 10.0 105 527 520 0.00 <2.5D 500 104 iO4 -4 cr-Civomium 25.5 25.7 99.2 <0.08 70.3 10.0 163 522 520 0.98 8.16 500 103 102 n Cu-Copper 132 124 106 <0-10 9.38 10.0 93.8 1681 1477 41.4 7085 500 119 78.2 Mo-Molybdenum 18.6 18.0 103 <0-10 10.3 10.0 103 505 508 0.99 75.00 500 101 T02 = Ni-Nickel 24.7 24.0 103 <0.05 10.6 10.0 106 534 531 0.95 6.D2 500 TO6 105 r Pb-Lead --- 26.5 27.1 97.8-- <0.n tO,7 -10.0 107- 538 633- - 0.96 10.7- 500- 105- - - SO4 Se Selen)um 50.5 67.0 75.4 <0.15 10,3 10.0 303 505 508 0.99 77.50 500 101 702 TI-Thal9um 86.1 88.4 97.4 <0.20 10.5 10.0 105 509 513 0.98 710.0 500 102 103 V-Vanadium 38A 38-6 98.4 <0.06 9.61 70-0 96.1 485 485 0.06 3.86 500 96.2 98.2 2n-Zinc 147 141 100 70.10 iO.S i0.O 305 642 650 0.95 118 500 105 iOfi V2.78 quid DC Sample Reagent Inorganic Ventures Duplicate Spiked Sample HML No.: AN00468 Matrix: uauID a Blank Reference Standard F Element m Spike Results= 91k3 mglL P rngJkg Unspiked Spike % Recovery known % found known % A: B: APD Result Added mgR (mglkg) (mg/kg) A: B: U As-Arsenic 2.63 106 <0.10 1.03 1.00 703 10T 10T O.B9 72.00 100 102 101 A8a-Barium 9.92 100 <0.010 0.98 1.00 98.0 97.3 97.0 0.3t 0.24 T0O 97,7 98.Hcc Ba-Be ilium 2.97 98.0 <0.005 0.20 0.20 100 20.2 20.1 1-00 70.16 20.0 i0i 100 m w Cd-Cadmium 3.32 3.TO 107 <0,010 1.05 1,00 105 707 106 0.94 70.20 100 107 708 0i Co-Cobalt 2.76 2.66 104 <0-05 1.03 1.00 103 105 105 0.00 <1.00 100 105 105 CR p U Cr-Chromium 15-7 15.0 105 70.08 i.O3 1.00 153 104 TO3 0.97 <1.6D 100 104 103 0 cu-Copper 65.9 66,1 99.7 <0.30 0.95 1.00 95,0 T56 155 1.05 80.4 tOD 85.6 94.6 m Mo-Mol enum 6.91 6.36 109 <0.10 1.04 1.00 104 110 110 0,00 6.64 100 I03 103 ¢ Y N r icke] 12.2 11.7 ]04 <0.05 1.04 i.0O 104 107 706 0.94 71.00 I00 107 106 to M Pb-Lead 6.07 6,18 111 <0.10 1.05 1.00 105 106 105 0.95 <2.00 700 106 105 N Se-Salanium 14.6 14.1 104 <0.16 7.03 3.00 103 103 102 0.98 73.00 100 ]03 102 TI-Thallium 36.2 34.5 105 <0.20 1.04 1.00 104 704 104 0.00 <4.00 100 104 104 m V-Vanadium 2.29 2.33 96.3 70.08 0.97 1.00 97.0 96.9 98.3 0.62 71.20 t00 96.9 96.3 N Znc 25-6 24.4 705 <O.(0 1.03 t.OD ID3 113 112 0.95 7,25 100 106 105 v �:P Analyst's Signature: dV � �/ Jamail Garche, Su enrTsor: Aa'!t/✓iJ pate. 03 -4 v:hemist: Fatima Huss C misf s ignatore:�A7inr�r 7•J7,QC4 y„� P fV orate Analyzed: 1012T103