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Ge•Analytical Laboratorie•Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# M170-10 8010B Date: 6/25/01 <br /> Date Rec'd: 6/19/01 <br /> Thorpe Oil Project: City of Stockton-Cineplex Project Date Started: 6/22/01 <br /> PO Box 357 Date Completed: 6/25/01 <br /> Lodi CA 95241 PO# <br /> Date Sampled: 6/19/01 <br /> Time: <br /> Sampler : R Azevedo(Geo) <br /> Sample ID: Stock Pile @ West End <br /> Lab ID: M202125 <br /> Method RL Analyte Results Units <br /> 8010B 167 Bromodichloromethane ND pg/Kg <br /> 167 Bromoform ND <br /> 167 Bromomethane ND <br /> 167 Carbon Tetrachloride ND <br /> 167 Chlorobenzene ND <br /> 167 Chloroethane ND <br /> 167 2-Chloro ethyl vinyl ether ND <br /> 167 Chloroform ND <br /> 167 Chloromethane ND <br /> 167 Dibromochloromethane ND <br /> 167 1,2-Dichlorobenzene ND <br /> 167 1,3-Dichlorobenzene ND <br /> 167 1,4-Dichlorobenzene ND <br /> 167 Dichlorodifluoromethane ND <br /> 167 1,1-Dichloroethane ND <br /> 167 1,2-Dichloroethane ND <br /> 167 1,1-Dichloroethene ND <br /> 167 trans-1,2-Dichloroethene ND <br /> 167 1,2-Dichloropropane ND <br /> 167 cis-1,3-Dichloropropene ND <br /> 167 trans-1,3-Dichloropropene ND <br /> 167 Methylene Chloride ND <br /> 167 1,1,2,2-Tetrachloroethane ND <br /> 167 Tetrachloroethene ND <br /> 167 1,1,1-Trichloroethane N D <br /> 167 1,1,2-Trichloroethane ND <br /> 167 Trichloroethene ND <br /> 167 Trichlorofluoromethane ND <br /> 167 Vinyl Chloride ND <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 3330 4363 131.0 66-133 <br /> 2-Bromo-l-chloropropane 3330 3380 101.5 63-139 <br /> 4-Bromofluorobenzene 3330 3380 101.5 64-136 <br /> Elevated detection limits due to matrix interference. <br /> L&O <br /> Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />