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titieurofins <br />Calscience <br />Analytical Report <br />Page 9 of 28 <br />Cardno ERI Date Received: 02/10/15 <br />601 North McDowell Blvd. Work Order: 15-02-0688 <br />Petaluma, CA 94954-2312 Preparation: EPA 5030C <br />Method: EPA 8260B <br />Units: ug/L <br />Project: ExxonMobil 99CAS/022789C Page 3 of 4 <br />Client Sample Number <br />Lab Sample Date/Time Matrix Instrument Date <br />Number Collected Prepared <br />15-02-0688.4-A 02!06115 Aqueous GC1MS T 02/12/15 <br />11:50 <br />Date/Time QC Batch ID <br />Analyzed <br />02113/15 150212L050 <br />01:54 <br />Parameter <br />Result <br />RL <br />DF Qualifiers <br />Benzene <br />140 <br />50 <br />100 <br />Toluene <br />3100 <br />50 <br />100 <br />Ethylbenzene <br />760 <br />50 <br />100 <br />p/m-Xylene <br />7400 <br />50 <br />100 <br />Xylenes (total) <br />13000 <br />50 <br />1.00 <br />Methyl -t -Butyl Ether (MTBE) <br />ND <br />50 <br />100 <br />Tert-Butyl Alcohol (TBA) <br />ND <br />500 <br />100 <br />Diisopropyl Ether (DIPE) <br />ND <br />50 <br />100 <br />Ethyl -t -Butyl Ether (ETBE) <br />ND <br />50 <br />100 <br />Tert-Amyl-Methyl Ether (TAME) <br />ND <br />50 <br />100 <br />1,2-Dibromoethane <br />ND <br />50 <br />100 <br />1,2-Dichloroethane <br />ND <br />50 <br />100 <br />Surrogate <br />Rec. % <br />Control Limits <br />Qualifiers <br />1,4-Bromofluorobenzene <br />95 <br />68-120 <br />Dibromofluoromethane <br />91 <br />80-127 <br />1,2-Dichloroethane-d4 <br />89 <br />80-128 <br />Toluene -d8 <br />98 <br />80-120 <br />W-39-EX2 <br />154m4m-&B 02105/15 <br />Aquroas 00,'rAS L <br />0211,41151 42/14945 150214L014 <br />11:50 <br />20:00 <br />Parameter <br />Result <br />RL <br />DF Qualifiers <br />o -Xylene <br />5900 <br />100 <br />200 <br />Surrogate <br />Rec. <br />Control Limits <br />Qualifiers <br />1,4-Bromofluorobenzene <br />96 <br />68-120 <br />Dibromofluoromethane <br />97 <br />80-127 <br />1,2-Dichloroethane-d4 <br />101 <br />80-128 <br />Toluene -d8 <br />101 <br />80-120 <br />RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit. <br />7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501 <br />