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Page 14 of 38 <br /> Zalscience <br /> � �k'C %14 h C p p''o�f <br /> n vironmental <br /> �= Analytical Report <br /> 10 <br /> U <br /> aboratories, Inc. w <br /> Cardno ERI Date Received: 12/03/11 <br /> 601 North McDowell Blvd. Work Order No: 11-12-0206 <br /> Petaluma, CA 94954-2312 Preparation: EPA 5030C <br /> Method: EPA 8260B <br /> Units: ug/L <br /> Project: ExxonMobil 99CAS/022789C Page 4 of 6 <br /> Lab Sample Datelrime Dale Datelrime <br /> Client Sample Plumber Number Collected Matrix Instrument prepared Analyzed QC Batch ID <br /> W-33-3W2 1142-0206-10,A 12/01/11 Aqueous GCIMS L 12105/11 12/05/11 1112051-01 <br /> 07:55 19:29 <br /> Parameter Result RL DF Qual Parameter Result RL DF Qual <br /> Benzene 170 20 40 Diisopropyl Ether(DIPE) ND 0.50 1 U <br /> Toluene 570 20 40 Ethyl-t-Butyl Ether(ETBE) ND 0.50 1 U <br /> Ethylbenzene 25 0.50 1 Tert-Amyl-Methyl Ether(TAME) ND 0.50 1 U <br /> Xylenes(total) 140 20 40 1,2-Dibromoethane ND 0.50 1 U <br /> Methyl-t-Butyl Ether(MTBE) ND 0.50 1 U 1,2-Dichloroethane ND 0.50 1 U <br /> Tert-Butyl Alcohol(TBA) ND 5.0 1 U <br /> Surroaates: REC("/ol C4ntrol 911KI Surroaates: REC(%) Control <br /> mits �W <br /> Li <br /> Limits <br /> 1,4-Bromofluorobenzene 97 68-120 Dibromofluoromethane 98 80-127 <br /> 1,2-Dichloroethane-d4 102 80-128 Toluene-d8 99 80-120 <br /> W-34-DW3 11-12-0206-11-A 12/01/11 Aqueous GCIMS L 12105/11 12/05/11 1112051-01 <br /> 09:50 19:58 <br /> Parameter Result RL pEQual Parameter Result 51 a Qual <br /> Benzene 330 25 50 Diisopropyl Ether(DIPE) ND 0.50 1 U <br /> Toluene 690 25 50 Ethyl-t-Butyl Ether(ETBE) ND 0.50 1 U <br /> Ethylbenzene 34 25 50 Tert-Amyl-Methyl Ether(TAME) ND 0.50 i U <br /> Xylenes(total) 200 25 50 1,2-Dibromoethane 0.82 0.50 1 <br /> Methyl-t-Butyl Ether(MTBE) 11 0.50 1 1,2-Dichloroethane 1.0 0.50 1 <br /> Tert-Butyl Alcohol(TBA) ND 5.0 1 U <br /> Surrogates: REC M Control Qual Surrogates: REC(%) Control Qu <br /> al <br /> Lisrak Limrts <br /> 1,4-Bromofluorobenzene 98 68-120 Dibromdluoromethane 96 80-127 <br /> 1,2-Dichloroethane-d4 101 80-128 Toluene-i8 103 80-120 <br /> W-33-DW4 11-12-0206-12.8 11/30/11 Aqueous GC/MS L 12/06111 12/06/11 1112061.01 <br /> 10:15 12:15 <br /> Parameter Result RL DF Qual Parameter Result RL DF Qual <br /> Benzene 3.1 0.50 1 Diisopropyl Ether(DIPE) ND 0.50 1 U <br /> Toluene 6.4 0.50 1 Ethyl-t-Butyl Ether(ETBE) ND 0.50 1 U <br /> Ethylbenzene 2.6 0.50 1 Tert-Amyl-Methyl Ether(TAME) ND 0.50 1 U <br /> Xylenes(total) 7.9 0.50 1 1,2-Dibromoethane ND 0.50 1 U <br /> Methyl-t-Butyl Ether(MTBE) ND 0.50 1 U 1,2-Dichloroethane ND 0.50 1 U <br /> Tert-Butyl Alcohol(TBA) ND 5.0 1 U <br /> Surrogates: REC(%) Control Qual Surrogates: REC("/o) Control Qual <br /> Limits Limits <br /> 1,4-Bromofluorobenzene 105 68-120 Dibromo(luoromethane 101 80-127 <br /> 1,2-Dichloroethane-d4 113 80-128 Toluene-d8 104 80-120 <br /> RL-Reporting Limit DF-Dilution Factor Qua[-Qualifiers <br /> 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714)895-5494 FAX: (714)894-7501 <br />