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:Iient Sample Number Nurnper Gouecteo -- _-._..__.._ <br />V-DSCHG 12-06-0513-1-A 06/06/12 Air GCIMS V N/A 06/08112 12060OLOI <br />11:00 18:04 <br />Comment(s): <br />-The method has been modified to use Tedlar Bags instead of Summa canisters and is not NY NELAC accredited. <br />Page 3 of 11 <br />alsd nce <br />Result <br />,,, nCC000. <br />DF Qual <br />Parameter <br />`a <br />ti mfr <br />nvlronmenta/ <br />Analytical Report <br />0.0021 <br />0.0016 <br />1 <br />Xylenes (total) <br />■Ir aboratorres, Inc. <br />0.0087 1 <br />Toluene <br />Cardno ERI <br />Date Received: <br />06/08/12 <br />601 North McDowell Blvd. <br />Work Order No: <br />12-06-0513 <br />Petaluma, CA 94954-2312 <br />Preparation: <br />N/A <br />1 <br />Method: <br />EPA TO-15M <br />Surrogates: <br />Units: <br />mg/m3 <br />Project: ExxonMobil 99CAS/022789C <br />Qual <br />Page 1 of 1 <br />REC % <br />Lab Sample Date/Time <br />Matrix <br />Date Date/Time <br />InOrnment o-,.-..,. .. A A1—A QC Batch ID <br />:Iient Sample Number Nurnper Gouecteo -- _-._..__.._ <br />V-DSCHG 12-06-0513-1-A 06/06/12 Air GCIMS V N/A 06/08112 12060OLOI <br />11:00 18:04 <br />Comment(s): <br />-The method has been modified to use Tedlar Bags instead of Summa canisters and is not NY NELAC accredited. <br />Parameter <br />Parameter <br />Result <br />RL <br />DF Qual <br />Parameter <br />Result <br />RL DF Qual <br />Benzene <br />0.0021 <br />0.0016 <br />1 <br />Xylenes (total) <br />0.44 <br />0.0087 1 <br />Toluene <br />0.080 <br />0.019 <br />1 <br />Methyl -t -Butyl Ether (MTBE) <br />0.0090 <br />0.0072 1 <br />Ethylbenzene <br />0.063 <br />0.0022 <br />1 <br />Surrogates: <br />Surrogates: <br />REC % <br />Control <br />Qual <br />Surrogates: <br />REC % <br />Control Qual <br />Limits <br />Limits <br />Limits <br />Limits <br />1,4-Bromofluorobenzene 109 <br />57-129 <br />1,2-Dichloroethane-d4 <br />108 <br />47-137 <br />Tnl„endAQ <br />97 <br />78-156 <br />V -INF -OXO 12-06-0513-2-A 06106/12 Air GCIMS V NIA 06/08/12 12060811-01 <br />11:15 20:28 <br />Comment(s): -The method has been modified to use Tedlar Bags instead of Summa canisters and is not NY NELAC accredited. <br />RL <br />Parameter <br />Result <br />RL <br />DF Qual <br />Parameter <br />Result <br />RL DF Qual <br />Benzene <br />016 <br />0.16 <br />100 <br />Xylenes (total) <br />210 <br />4.3 500 <br />Toluene <br />77 <br />9.4 <br />500 <br />Methyl -t -Butyl Ether (MTBE) <br />ND <br />0.72 100 U <br />Ethylbenzene <br />36 <br />1.1 <br />500 <br />Surrogates: <br />REC % <br />Control <br />Qual <br />Surrogates: <br />REC % <br />Control Qual <br />Limits <br />Limits <br />1,4-Bromofluorobenzene <br />109 <br />57-129 <br />1,2-Dichloroethane-d4 <br />106 <br />47-137 <br />Toluene -d8 <br />96 <br />78-156 <br />Method Blank <br />099-12-983-2,366 <br />NIA Air GC/MS V <br />N/A <br />06/08/12 12060811-01 <br />13:12 <br />Parameter <br />Benzene <br />Toluene <br />Ethylbenzene <br />Surrogates: <br />1,4-Bromofluorobenzene <br />Toluene -d8 <br />Result <br />RL <br />DF Qual <br />ND <br />0.0016 <br />1 U <br />ND <br />0.019 <br />1 U <br />ND <br />0.0022 <br />1 U <br />REC % <br />Control <br />Qual <br />Limits <br />104 <br />57-129 <br />101 <br />78-156 <br />Parameter <br />Xylenes (total) <br />Methyl -t -Butyl Ether (MTBE) <br />Surrogates: <br />1,2-Dichloroethane-d4 <br />RL -Reporting Limit DF - Dilution Factor Qual - Qualifiers <br />Result RL DF Qual <br />ND 0.0087 1 U <br />ND 0.0072 l U <br />REC % Control Qual <br />Limits <br />109 47-137 <br />7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 • FAX: (714) 894-7501 <br />