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Lab Sample Date/Time Date Daterrime <br />RA+A- 1—+.,,..,e.,+ QC Batch Irl <br />Tient Sample Number Number Collected """ ^ . '� .." <br />'.• Meparee <br />u MI - Batch <br />V-DSCHG 12-03-1849-1-A 03/27/12 Air Gc/Ms 11 WA 03/28/12 1203281-01 <br />13:40 16:10 <br />Comment(s): <br />-The method has been modified to use Tedlar Bags instead of Summa canisters and is not NY NELAC accredited. <br />Page 3 of 10 <br />Caiscionce <br />Result <br />ut <br />ronmental <br />Analytical Report <br />rrL <br />° <br />r' <br />p <br />0.045 <br />0.0016 1 <br />., <br />I aboratodas, Inc. <br />0.0087 1 <br />Toluene <br />1.3 <br />0.075 4 <br />Methyl -t -Butyl Ether (MTBE) <br />Card -Z ERI <br />Date Received: <br />03/28/12 <br />601 North McDowell Blvd. <br />Work Order No: <br />12-03-1849 <br />Petaluma, CA 94954-2312 <br />Preparation: <br />N/A <br />RE % <br />Method: <br />EPA TO -15M <br />REC % <br />Units: <br />mg/m3 <br />Project: ExxonMobil 99CAS/022789C <br />Limits <br />Page 1 of 1 <br />Lab Sample Date/Time Date Daterrime <br />RA+A- 1—+.,,..,e.,+ QC Batch Irl <br />Tient Sample Number Number Collected """ ^ . '� .." <br />'.• Meparee <br />u MI - Batch <br />V-DSCHG 12-03-1849-1-A 03/27/12 Air Gc/Ms 11 WA 03/28/12 1203281-01 <br />13:40 16:10 <br />Comment(s): <br />-The method has been modified to use Tedlar Bags instead of Summa canisters and is not NY NELAC accredited. <br />DF Qual <br />Parameter <br />Result <br />RL DF Qual <br />Parameter <br />Result <br />RL DF Qual <br />Benzene <br />0.045 <br />0.0016 1 <br />Xylenes (total) <br />1.2 <br />0.0087 1 <br />Toluene <br />1.3 <br />0.075 4 <br />Methyl -t -Butyl Ether (MTBE) <br />ND <br />0.0072 1 U <br />Ethylbenzene <br />022 <br />0.0022 1 <br />Ethylbenzene <br />48 <br />0.35 <br />Surroaates: <br />RE % <br />Control Qual <br />Surroaates: <br />REC % <br />Control Qual <br />Control <br />Qual <br />Limits <br />REC °° <br />Control Qual <br />Li its <br />1,4-Bromofluorobenzene 110 <br />57-129 <br />1,2-Dichloroethane-d4 <br />91 <br />47-137 <br />Trdtrena-dS <br />65 <br />78-156 AZ <br />1,2-Dichloroethane-d4 <br />92 <br />V -INF -OXO 12-03.1849.2-A 03127112 Air GC1MS 11 NIA 03/28/12 120328LOI <br />13:45 17:44 <br />Comment(s): <br />-The method has been modified to use Ted lar Bags instead of Summa canisters and is not NY NELAC accredited. <br />DF Qual <br />Parameter <br />Result <br />RL <br />DF Qual <br />Parameter <br />Result <br />RL DF Qual <br />Benzene <br />5.0 <br />0.26 <br />160 <br />Xylenes (total) <br />260 <br />6.9 800 <br />Toluene <br />240 <br />15 <br />800 <br />Methyl -t -Butyl Ether (MTBE) <br />ND <br />1.2 160 U <br />Ethylbenzene <br />48 <br />0.35 <br />160 <br />REC ° Control Qua] <br />Limits <br />Surroaates: <br />REC °° <br />Control <br />Qual <br />Surroaates: <br />REC °° <br />Control Qual <br />1,2-Dichloroethane-d4 <br />97 <br />Limits <br />Toluene -d8 <br />89 78-156 <br />Limits <br />1,4-Bromofluorobenzene 108 <br />57-129 <br />1,2-Dichloroethane-d4 <br />92 <br />47-137 <br />Toluone-d8 <br />81 <br />78-156 <br />Method Blank 099.12-983-2,212 NIA Air GCIMS II NIA 03/28/12 120328L01 <br />113:35 <br />Parameter <br />Result RL <br />DF Qual <br />Parameter <br />Result <br />RL DF Qual <br />Benzene <br />ND 0.0016 <br />1 U <br />Xylenes (total) <br />ND <br />0.0087 1 U <br />Toluene <br />ND 0.019 <br />1 U <br />Methyl -t -Butyl Ether (MTBE) <br />ND <br />00072 1 U <br />Ethylbenzene <br />ND 0.0022 <br />1 U <br />Surroaates: <br />REC (%) Control <br />Q al <br />Surroaates: <br />REC ° Control Qua] <br />Limits <br />Limits <br />1,4-Bromofluorobenzene <br />102 57-129 <br />1,2-Dichloroethane-d4 <br />97 <br />47-137 <br />Toluene -d8 <br />89 78-156 <br />RL -Reporting Limlt , OF - Dilution Factor dual - Qualifiers <br />7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 - FAX. (714) 894-7501 <br />