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POSITItE !IMMM Pr LAB SERVICE 781 East Washington Blvd., Los Angeles, CA 90021 (213) 745-5312 FAX (213) 745-6372 Certificate of Analysis Page z of z --+.-« Pacific Resource Recovery File #:73862 3150 E. Pico Blvd. Reported: 09/21/06 15:23 Los Angeles, CA 90023 Submitted: 09/12/06 Attn: Ben Obiaga Phone: (323)261-7145 FAX:(323) 780-0078 PLS Report No.: 6090069 Project: Interstate Truck Center No. B/S 93181 PO No. 3966 Sampfe ID:. B/5 93181 Booth F11 Solid (6090069-0Y) Sampled:09/12/06 13:10 Received:09/12/06 13:52 Anal - Results Flag D.F. Units P e , - . _ l _ Q_ _ Prep/Test Method Prepared _Analyzed _By_Batch_ 1,1,2,2-Tetrachloroethane ND 4 ug/kg 16.0 EPA 5030B EPA 82608 - 09/19/06 09/19/06 ai B162013 1,2,3-Trlchloropropane ND 4 , ug/kg 16.0 EPA 50308 EPA 82608 09/19/06 09/19/06 al 8162013 n-Propylbenzene ND 4 ug/kg 16.0 EPA 5030B EPA 82608 09/19/06 09/19/06 al 8162013 2-Chlorotoluene ND 4 ug/kg 16.0 EPA 50308 EPA 82608 09/19/06 09/19/06 al 8162013 4-Chlorotoluene ND 4 ug/kg 16.0 EPA 5030B EPA 82608 09/19/06 09/19/06 al 8162013 1,3,5-Trlmethylbenzene ND 4 ug/kg 16.0 EPA 50308 EPA 82608 09/19/06 09/19/06 ai B162013 tert-Butylbenzene ND 4 ug/kg 16.0 EPA 5030B EPA 8260B 09/19/06 09/19/06 ai B162013 1,2,4-Trimethylbenzene 41.5 4 ug/kg 16.0 EPA 50308 EPA 82608 09/19/06 09/19/06 ai BI62013 sec-Butylbenzene ND 4 ug/kg 16.0 EPA 5030B EPA 82608 09/19/06 09/19/06 al 8162013 1,3-Dlchlorobenzene ND 4 ug/kg 16.0 EPA 50308 EPA 82608 09/19/06 09/19/06 al B162013 4-1sopropyltoluene ND 4 ug/kg 16.0 EPA 5030B EPA 82608 09/19/06 09/19/06 al BI62013 1,4-Dichlorobenzene ND 4 ug/kg 16.0 EPA 50308 EPA 82608 09/19/06 09/19/06 ai BI62013 1,2-Dichlorobenzene ND 4 ug/kg 16.0 EPA 5030B EPA 82608 09/19/06 09/19/06 al 8162013 n-Butylbenzene ND 4 ug/kg 16.0 EPA 50308 EPA 82608 09/19/06 09/19/06 al BI62013 1,2-Dlbromo-3chloropropane(DBCP) ND 4 ug/kg 16.0 EPA 5030B EPA 82608 09/19/06 09/19/06 ai 6162013 1,2,4-Trichlorobenzene ND 4 ug/kg 16.0 EPA 50308 EPA 82608 09/19/06 09/19/06 al BI62013 w.�.. Hexachlorobutadlene - -•----+- •-.- 141'-�+...-,„,,,.,_ug/kg- 16:0�,-EPA 503013--EPA 82606-09/19/D6�,09/19/06- -al0-Bl62013 Naphthalene 34.6 4 ug/kg 16.0 EPA 50308 EPA 82608 09/19/06 09/19/06 al 8162013 1,2,3-Trichlorobenzene ND 4 ug/kg 16.0 EPA 5030B EPA 82608 09/19/06 09/19/06 al B162013 Methyl tert-butyl ether(MTBE) ND 4 ug/kg 16.0 EPA 50308 EPA 8260B' 09/19/06 09/19/06 al BI62013 1,4-Dioxane ND 4 ug/kg 320 EPA 50308 EPA 82608 09/19/06 09/19/06 al 8162013 __- .. _- .___.__ __ ... _. . Surrogate:4-Brom0luorobenzene 84.8% 82-122 EPA 50308 EPA 82608 09/19/06 09/19/06 a/ 8162013 Surrogate:Toluene-d8 88.3% 76-117 EPA 5030B EPA 82608 09/19/06 09/19106 ai B162013 Surrogate:Dlbromofiuoromethane 56.3% 71-151 EPA 50308 EPA 8260B 09119/06 09/19/06 al 8162013 Arsenic ND 1 mg/kg 1.00 EPA 30508 EPA 60308 09/13/06 09/13/06 barium 365 1 mg/kg 1.00 EPA 30508. EPA 6010B 09/13/06 09/13/06 9 8161415 g/ g h 8161415 Cadmium ND 1 mg/kg 1.00 EPA 30500 EPA 60108 09/13/06 09/13/06 Chromium 47.4 1 m 1.00 EPA 30508 EPA 60108 09 13 06 09/13/06 h BI61415 �k g / / Cl 8161415 Lead 135 1 mg/kg 0.500 EPA 30508 EPA 60108 09/13/06 09/13/06 h 8161415 Selenium ND 1 mg/kg 1.00 EPA 30500 EPA 60108 09/13/06 09/13/06 cJ 8161415 Silver ND 1 mg/kg 1.00 EPA 30508 EPA 60108 09/13/06 09/13/06 cJ BI61415 Mercury ND . . , �.am.«,v.....,...... ..ncc,,.:. 1 mg/kg 0.100 EPA 7471A EPA 7471A 09/13/06 09/13/06 dip B161403 Notes and Definitions /' NA Not Applicable ND Analyte NOT DETECTED at or above the detection limit NR Not Reported MDL Method Detection Limit PQL(RL) Practical Quantitation Limit(RL) Authorized Signature(s) I Estimated concentration detected between MDL and PQL values. . Environmental Laboratory Accreditation Program Certificate No. 1131, Mobile Lab No.2534,LACSD No. 10138