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,L GeoAnalytical Laboratories, Inc. 1405 Kansas Avenue Modesto,CA 95351 Certification#2585 Phone(209)572-0900 Fax(209)572-0916 Report# USC1905 Project: Sand Blasting Area Bate: 03/25/08 San Joaquin County Environmental Health Date Ree'd: 03/19/08 600 East Main St PO#: Stockton,CA 95202 Inorganic Chemistry-Quality Control GeoAnalytical Laboratories, Inc. Reporting Spike Source %REC RPD Llvte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch U000861 -3050B Prepared: 03/21/08 Analyzed: 03/24108 LCS Aup(U000861-BSDI) Antimony 5.13 0.5 mg/kg 5.000 103 80-120 14 20 Arsenic 5.27 0.5 5.000 105 80-120 2 20 Barium 13.4 0.5 12.50 107 80-120 0.07 20 Beryllium 4.86 0.5 5.000 97 80-120 4 20 Cadmium 5.25 0.5 5.000 105 80-120 0.8 20 Chromium 5.31 0.5 5.000 106 80-120 6 20 Cobalt 5.52 0,5 5.000 110 80-120 5 20 Copper 6.00 0.5 5.000 120 80-120 0 20 Lead 4.80 1.0 5.000 96 80-120 3 20 Molybdenum 5.76 0,5 5.000 115 80-120 0 20 Nickel 5.68 0.5 5.000 114 80-120 3 20 Selenium 4.76 0.5 5.000 95 80.120 0 20 Silver 56.6 1.0 50.00 113 80-120 3 20 Thallium 4.60 0,5 5.000 92 80-120 0.7 20 Vanadium 13.3 0.5 12.50 107 80-120 10 20 Zinc 5.73 0.5 5.000 115 80-120 3 20 Mercury 1.40 0.5 1.250 112 80-120 6 20 Matrix Spike(U000861-MSI) Source:U8C1905-03 Antimony 4.84 0.5 mg/kg 5.000 ND 97 80-120 Arsenic 5.49 0.5 5.000 0.93 91 80-120 Barium 117 0.5 12.50 160 NR 80-120 QM-02 Beryllium 5.07 0.5 5.000 ND 101 80-120 Cadmium 5.33 0.5 5.000 ND 107 80-120 Chromium 9.51 0.5 5.000 5.50 80 80-120 Cobalt 5.68 0.5 5.000 L22 89 80-120 Copper 16.4 0.5 5.000 7.20 184 80-120 QM-02 Lead 10.7 1.0 5.000 6.93 75 80-120 QM-02 Molybdenum 5,26 0.5 5.000 0.82 89 80-120 N ickel 7.24 0.5 5.000 3.20 81 80-120 Selenium 4.68 0.5 5.000 ND 94 80-120 Silver 21.7 1.0 50.00 6.37 31 80-120 QM-02 Thallium 3.88 0.5 5.000 ND 78 80-120 QM-01 Vanadium 16.4 0.5 12.50 4.36 96 80-120 Zinc 314 0.5 5,000 299 291 80-120 QM-02 Mercury 0.96 0.5 1.250 ND 77 80-120 QM-01