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4. Procedure <br /> When soil is ready to be sampled, the field staff person shall perform the following <br /> activities, not necessarily in the order listed. <br /> Soil Sampling Activities <br /> If the excavation is less than 5 feet deep and the field staff person is comfortable with the <br /> site conditions,the excavation may be entered to obtain samples directly from the <br /> sidewalls/bottom. If the excavation is 5 feet or deeper, the field staff person will not enter <br /> the excavation without direction from a "competent person" and/or adequate shoring <br /> (pursuant with OSHA requirements). <br /> • Soil shall be obtained from the desired location by means of the excavation <br /> equipment at the site (backhoe/excavator bucket), drill rig or hand auger, and brought <br /> to the ground surface for access.Near the teeth of the backhoe bucket, or at the <br /> bottom of the sample liner, soil will be scraped away using a clean trowel or other <br /> clean device. A clean brass or stainless steel sleeve, glass jar or En Core®sampler will <br /> then be pushed directly into the uncovered soil until full, or a new plastic 10 ml <br /> syringe will have the bottom end removed, and the syringe will be inserted into the <br /> exposed soil until approximately five milliliters of soil is collected. <br /> • Soil samples will be collected in one of three ways, depending on the constituents the <br /> laboratory will be requested to analyze for. <br /> 1. For laboratory analysis of non Volatile Organic Compounds(VOCs), soil samples <br /> will be collected with laboratory supplied glass jars or clean brass or stainless steel <br /> sleeves. A six-inch filled sleeve of the sample will be capped with Teflon sheeting <br /> and plastic end caps, labeled, and sealed in a plastic storage bag. Glass jars are sealed <br /> with the supplied screw-lid after filling the jar. Sample numbers and sample time will <br /> be noted. Each sample will then be placed in an ice chest(chilled to 4°C)until <br /> delivered to a state-certified laboratory under chain-of-custody documentation. <br /> 2. For laboratory analysis of VOCs, soil samples will be collected using an En <br /> Core sampler. As per EPA Method 5035, a new disposable En Core Sampler <br /> will be placed in the En Core®handle. Three clean En Core® sample tubes will be <br /> driven into the soil adjacent to each other and filled completely to avoid air space. <br /> The En Core® sample tube will be retracted from the soil and capped with the <br /> locking cap, and inserted in the provided envelope. Each envelope will be labeled <br /> with the job number,the sample identification, date and time of collection,the <br /> sampler's name, and the analyses required. Each set of three En Core®samples <br /> will then be placed in an ice chest(chilled to 4°C) until delivered to a state- <br /> certified laboratory under chain-of-custody documentation, where they will weigh <br /> and preserve each sample within 48-hours of collection. A glass jar or sleeve will <br /> also be collected for laboratory screening or additional analyses, by capping a <br /> sample sleeve with Teflon sheeting, and tight-fitting plastic caps, or sealing the <br /> jar with the provided lid, and including it with the samples as described in <br /> Sections I and 3. <br /> SOP Soil Sampling for 5035 VOCs 2 Of 5 August 2011 <br />