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GGIMS MetbaEA GC Memotls <br /> G ams Methods OC MetlaJe Mod led COMMENTS <br /> Modl/letl Modified Modified Modified COMMENTS Method? Modifatl USEPA TO- Matlilietl MotliOetl Modaetl <br /> Mender MatlIReG USEPA ed Parameter USEPA/360 USEPAT047 USEPAOUtS USEPA 0031 <br /> To <br /> Paameter UBEPA0200 USEPATO-1T USEPA 0016 USEPA 0021 16 <br /> 16 1.Melpicel <br /> See forma as <br /> One per zn One per 20 One per 20 One per 20 gppandlx F p.USEPA <br /> One per 20 samples samper or sampbs of samples or samples or 0Nls TO-15. <br /> DUPBceree a batch.wM1kM1ever bathe. brim, batch, batch g3Wance la <br /> Is more ohm. ,dCowr is Anchor.is wWcheverls =own a tllscair 2amilyTbn <br /> more ohee. moreo0m. masa man. mase ahen. %RPD"25%. InshlyylayoU <br /> � Newt swMm <br /> One per 20 Ore p.20 One par 30 One per 20p, A F odea <br /> One Per 20 samples samples eamPdsce sareplasa pal a " ppas Wx 3nd1 lWct and Use only To odY ar <br /> Use 1 <br /> flePlleates wbatch wfikhaver Mlch Mont belch batch. �Ou 'distributed rouare ��owUa))YYtt00 <br /> is more ahen. whlclKvd is wddnv.Is whichever is vA11h Is NscWussebna t.Tudrg:50 Volume Pala- ^b^habg ai p "Ion at <br /> • <br /> me often. rrveoften. rmeohen. ft %RPDS5%. well <br /> Se InlJaltyand Iddaradd- chazarariza .Ized <br /> APPmdx F evwy 24 load sites. spas.Olhp"::.'salter. . <br /> "sexul,Oodral Opaorel Nd Req+Yetl Not RaquYetl. OpMnal Optional of Nis earn TPH„ <br /> Mass.Meet 4. DetxmNd of maficetby Idanllllcpilon <br /> samples(I-CS) If Wancefor eccapeme a1Wan'Safe ql naW of nal <br /> dissuasion. ulmfd es pa Sampling t ..,units <br /> See Tunbg:50 rg Tads 3d Volume' OnmPateol must be <br /> Sae See Ammar IF BromdluasaMmzma USEPA TO- (SSV)g most an mnNmed <br /> MBthotl Derecaan See AppmtlNFd Sea Appendix See Appendix pAebrdxF AppendixF afthH 15. psAg vas per conlYmetl either by <br /> I�FBI InYJeM antl <br /> F of this Fdthis olhls adels 12 Mass, 'either by second <br /> thatet.prding Umlt this gandome. Wena guidance. I d1worre la Other Requirements ery And <br /> second <br /> m gWJarce: guidance. discussbn. Meet erreperke 2.Must meet antl t3.t 2 til mlamn a dw.. a <br /> Sce Alma <br /> 4OfUSsp.20, eque"era USEPA TO defense deterty <br /> deeper4 d USEPA 8250, dryad.,and <br /> Raparting Elmd Oras ran be"of One per calm bac one of batebd r On.pre of AstldF In InS bn].2 Per USEPA as Nm laSd <br /> VadRCMion ampler. batch of of samples:. Nen 10%of therm <br /> samples.ora sampks.� samples. guidance la of T045 antl those <br /> '� rr <br /> excusable T0.15 to Swim 11,2 ympWs samples <br /> mb le <br /> M�Nnd blank Method blank ^pan Aside of USEPA mutba confirmed <br /> taNg fled T0.17 <br /> Mathnd No*using ftwnld0ed mads 0e0 T0. S:.Anatytical walpA wkfte <br /> humWMedlabgade As par As per Seca. left Bede IM Dade p. preclslore ted �g45 mCM15 <br /> Wa»pre aVas Sedim le] 107.1of Wire peaW aWapeaeY = as P.Samoa �nd .hnd. <br /> Mdhatl Banka sample and per of USEPA USEPA TO as zampla as sample 11.3.02 of <br /> AT <br /> Swim 0A.1 of TO 15. P. and per endpar USEPATO- <br /> Swim <br /> Sedan 9.5 Samoa 8.4 6. <br /> of USEPA dUSEPA p.lamanra <br /> Bm5C. 002E .a mdse a5 per <br /> One se'mpW One sample Ore sasbde One sample pn sample ��� Secaon 14 of <br /> capklmr r20 romaMw p. wM dank per mdaherpw codaN.P^+ g.e..nodded USEPA TO <br /> pe 20 samples w 20 samples as 20 samples 20 samples vales)d 17' <br /> Cantudd r Blank samplaS di Pa loss". per larch, a per betzM1. re per boom, sempirg <br /> bash,AbdulA NticM1ay.Is vaaclay.Is wWCMer iz wdcMver Is amen 11 <br /> .^lora°trans rmaoften. rmeobare. mdeman. ab aallen. e�M 'Adapted from"Guide to Environmental Analylical Methods"5A Edition,Edited by Roy-Keith Smith,Ph.D.. <br /> • .. '' . Meryon Malyze Genium Publishing Corp.,2003, <br /> analyze Andyae ASAP. ASAP, <br /> PMASAP ASAP. UP to ASAP. Upon samples Samples 11t Initial,Onedime,demonsbaUon of ability to generale acceptable accuracy and precision. Procedure <br /> Ilse 14 days try 3o aeys mkecnd b mkmed In may need to be repeated II changes In InsWment,methodology or personnel occur. USEPA Method <br /> 'Sempbs cgllacretlln samples in nMgerered. Arspread ®asandnd <br /> passiedetl ca apbx adeno ExcepMna as mos can nlstwscen 800013(Determinative Chromatographic Separations),Revision 2,December 199fi(SW-846 Manual). <br /> Holding Tabe canMMld up on" ccaabnHnrs. mea In MMkt up to MMhupm <br /> days.Tedium bag Target-Mg section 10.10 14 days. 14 days. tel Mid.ldyel NIST(National Institute of Standard and Technology)traceable(where available or <br /> use re discaaagetl. use is 0USEPA T6 Tadid®bag Transfrbag equivalent)vapor-phase standard. <br /> Wscwragee. tT. use Is bawls <br /> discona duow <br /> O1 No Internal standards and surrogates were suggested by the method. The compounds are to be <br /> selected by the analyst(lab)and they must be similar In analytical behavior to the compounds of interest. <br /> The analyst needs to demonstrate the internal Standards are not affected by method or matrix <br /> Interferences. <br /> to There Is no limit on the number of samples per batch for Reporting Limit Verification. Once per day Is <br /> suf9dent <br /> 3/3/2010 -39- 3/3/2010 -40- <br />